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  • Articles: DFG German National Licenses  (26)
  • Electronic Resource  (26)
  • 2005-2009  (26)
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  • Articles: DFG German National Licenses  (26)
Material
  • Electronic Resource  (26)
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  • 1
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Key engineering materials Vol. 359-360 (Nov. 2007), p. 409-413 
    ISSN: 1013-9826
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Ultrafine grain WC hardmetals were manufactured successfully from mixed powders ofnominal composition of WC-6Co-1.5Al(wt%). To manufacture bulk ultrafine grain WC alloys,nanocrystalline WC powders as precursor were prepared for sintering from the mixed commerciallyavailable powders by high energy milling of 15 h. Then the electrical current sintering process ofthe milled powders was further studied. Experimental results showed that the density, hardness andtransverse rupture strength of the sintered alloys reached 14.224 g/cm3, HRA 94 and 1660 MPa,respectively, by a appropriate coupling of pulse- and subsequent constant-current sintering and withthe total sintering time of 6 min. It seemed difficult to obtain desirable sintered hardmetal by asingle type of electric current sintering. However, the application of intensive pulse electric currentwas favorable to sintering, although it was difficult to achieve good WC alloys only by the pulseelectric current sintering. A higher density WC alloy could be prepared by enlarging the electriccurrent when only constant electric current was applied to sinter the milled powders. Unfortunately,the WC grains substantially coarsened concurrently so that the mechanical properties of the assintered alloy decreased obviously
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Key engineering materials Vol. 353-358 (Sept. 2007), p. 1621-1624 
    ISSN: 1013-9826
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Warm compacting and sintering behaviors of pre-mixed Fe-2Ni-2Cu-1Mo-1C powderswere studied. Results showed that green density increased with compacting temperature and thenfell slightly; the maximum green density was obtained at about 120°C. Green compact density andspring back effect of the pre-mixed powder increased gradually as the compacting pressureincreased. Sintered density first increased and then fell as the temperatures went up under differentsintering temperatures for 50 minutes, but the trends of sintering dilatation were first reduced andthen increased. Sintered density first reduced and then increased with the prolonged sintering timeat 1300°C, but the trends of dimension change after sintering were the very reverse. Tensile strength,elongation and hardness of the warm compacted Fe-2Ni-2Cu-1Mo-1C materials generally increasedas sintering temperature and sintering time went up
    Type of Medium: Electronic Resource
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  • 3
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Key engineering materials Vol. 353-358 (Sept. 2007), p. 2143-2146 
    ISSN: 1013-9826
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Constant current plus pulse current electrical sintering was introduced into the sinteringof a ball-milled nanocrystalline Fe-2Cu-2Ni-1Mo-0.8C mixed powder. Effect of pulse currentcharging time on the properties of sintered products was studied. Constant electric current sinteringwas also used for comparison. A nanostructured iron-based material was obtained within 4 minutesof sintering. It has a density of 7.7 g/cm3 (relative density of 98.7 %) with an average grain size(iron-matrix) of 58 nm and carbide particle size of less than 100 nm, a hardness of HRC 64 andtransverse rupture strength of 2004 MPa. When only pulsed electric current sintering was used witha sintering time of 5 min, a fine grained iron-base material with density of 7.74 g/cm3 (relativedensity of 99.2%), a hardness of HRC 65 and transverse rupture strength of 2045 MPa was obtained
    Type of Medium: Electronic Resource
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  • 4
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Key engineering materials Vol. 280-283 (Feb. 2007), p. 1559-1562 
    ISSN: 1013-9826
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Gypsum powders and calcium phosphate/gypsum powders were synthesized by wet method. The influences of the pH and temperature on the morphology of the gypsum crystal were studied by light microscopy. The effects of the initial calcium/phosphorus molar ratio and the pH of the solution on the microstructure and phase composition of the calcium phosphate/gypsum composite powders were studied by scanning electron microscopy and X-ray diffractometry. The results show that both temperature and pH value had influence on the crystal shape of gypsum and the pH value was the predominant parameter for the particle shape and phase composition of the composite powders
    Type of Medium: Electronic Resource
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  • 5
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Key engineering materials Vol. 353-358 (Sept. 2007), p. 813-816 
    ISSN: 1013-9826
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: By choosing appropriate annealing temperature and annealing time, diffusion couplesmade of aluminum bronze and tool materials were prepared to simulate the diffusion and phaseformation during the actual machining. These results were compared to those obtained from turningexperiments. In agreement with results obtained from diffusion couple experiments, all turningexperiments showed that major elements in both tool materials and workpiece diffused into theircounterparts. The diffusion of C away from the tool will reduce the tool strength. It is helpful to usediffusion couple results to comprehend the diffusion effect in the actual turning process
    Type of Medium: Electronic Resource
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  • 6
    ISSN: 1422-6375
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Nanohybrid thin films consisting of nanocrystalline TiO2 particles in poly(methyl methacrylate)(PMMA) were successfully synthesized by in-situ sol-gel and polymerization assisted by spin coating. Using titanium isoproproxide (Ti-iP), methyl methacrylate (MMA) and 3-(trimethoxysily)propyl methacrylate (MSMA) as the starting materials, nanohybrids containing up to 60% Ti-iP inPMMA were realized. The resulting nanohybrid thin films coated on quartz substrates are optically transparent and demonstrate nonlinear optical behaviour, where their nonlinear absorption increases with the loading of Ti-iP in PMMA, as confirmed by Z-scan measurements. Using pump-probe technique, these thin films are shown to exhibit an ultrafast relaxation time of ~1.5 picosecond
    Type of Medium: Electronic Resource
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  • 7
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Materials science forum Vol. 532-533 (Dec. 2006), p. 353-356 
    ISSN: 1662-9752
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: The fabrication of a large Al-4.5wt%Cu-0.5wt%Mn wheel with 670mm diameter byindirect squeeze casting process was studied. The casting system including modified hydraulic pressand die structure was introduced, and the casting procedures was designed and described. Thefilling behavior of the casting process was simulated with software Flow3D. It was found that whileflowing from spoke to rim, turbulence flow of liquid melt in the vicinity of free surface was found,and that at the end of the filling, the unwanted solidification might occur. To reduce the turbulentflow and the unwanted solidification, a modified injection condition was proposed. The simulationresults with the modified injection indicated that the turbulence was prevented and the unwantedsolidification during the filling was reduced as well. The squeeze wheel castings were fabricatedwith the modified injection condition. Cross sections of the castings were checked. A number ofspecimens were obtained from different parts of the castings to evaluate microstructure of the wheel,and both high density and fine grain microstructures were found in the specimens. Mechanicalproperties of the tensile samples from the wheels with T5 heat treatment were measured. Theaverage tensile strength and elongation were 390 MPa and 10%, respectively
    Type of Medium: Electronic Resource
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  • 8
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Materials science forum Vol. 534-536 (Jan. 2007), p. 1-4 
    ISSN: 1662-9752
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: In conventional studies, different empirical atomization equations are correlated fordifferent kinds of atomization methods or even in the same method. In the present study, it wasfound that the basic law of melt breakup from bulky liquid into droplets can be universally appliedto all atomization methods. Based on theoretical analysis, a new general equation of mean particlesize applicable to both conventional atomization methods and new atomization processes ispresented. The mean particle size in melt atomization is mainly controlled and decided by two keydimensionless parameter groups representing the liquid stability of melts and the breakup ability ofatomizer respectively. Different specific atomization mechanisms result in different formulae inconventional atomization methods. In case of gas atomization, it is equivalent with and can bechanged into Lubanska Equation. In case of centrifugal atomization, it can be changed into theequations that are currently the most widely used. In case of water atomization, it is similar to theequation proposed by Grandzol and Tallmadge. According to the universal equation, newcorrelations for mean particle size in novel atomization processes such as Hybrid Atomization andMultistage Atomization were proposed and agreed with our experimental data well
    Type of Medium: Electronic Resource
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  • 9
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Materials science forum Vol. 532-533 (Dec. 2006), p. 817-820 
    ISSN: 1662-9752
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: The rolling compaction can produce porous or dense strips with special functions. Themechanical behaviors in rolling compaction are hard to predict accurately and efficiently bytraditional means. The numerical simulation based on the Finite Element Method (FEM) provides aflexible and efficient way for such problems. This paper introduces three-dimensional (3-D) FEMsimulations for the rolling compaction of the iron matrix powders. The elliptical yield criterion,elasto-plastic constitutive relationship and the friction model were analyzed. Simulations werebased on the second-developed user subroutine in MSC.Marc. Effects of friction and rollingvelocity on the rolling force, distribution of the density and some other parameters were analyzed
    Type of Medium: Electronic Resource
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  • 10
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Materials science forum Vol. 534-536 (Jan. 2007), p. 589-592 
    ISSN: 1662-9752
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: A new process of pulsed electric current sintering was developed. It combinescompaction with activated sintering effectively and can manufacture bulky nano-crystallinematerials very quickly. Pulsed electric current sintering of high-energy ball-milled nano-crystallineiron-based powders is investigated in this work. A nanostructured steel is obtained with highrelative density and hardness by this process. The average grain size of iron matrix is 58nm and thecarbide particulate size is less than 100nm. The densification temperature of ball-milled powders isapproximately 200ºC lower than that of blended powders. When the sintering temperature increases,the density of as-sintered specimen increases but the hardness of as-sintered specimen firstincreases and then decreases. Microstructure analysis results show that the decrease of hardness iscaused by the dramatic grain growth of iron matrix
    Type of Medium: Electronic Resource
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