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  • Articles: DFG German National Licenses  (3)
  • 2005-2009  (3)
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  • Articles: DFG German National Licenses  (3)
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Year
  • 1
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Materials science forum Vol. 475-479 (Jan. 2005), p. 2131-2134 
    ISSN: 1662-9752
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Annealing effect on the magnetic properties of Fe-Pt nanoparticle was investigated. Fe-Pt nanoparticles were synthesized by the chemical reduction of H2PtCl6 and the decomposition of Fe(CO)5 in the presence of PVP polymers. The samples were annealed at several temperatures from 350℃ to 600℃ and the structural and magnetic properties were studied by TEM, XRD and magnetization measurements. FePt nanoparticles as-synthesized showed super-paramagnetism and annealed samples at temperatures more than 400℃, ferromagnetism. The crystal structure ofas-synthesized sample was disordered fcc, but chemically ordered fct, when it was annealed at more than 400℃. The annealing effects are the concatenation or agglomeration of nanoparticles accompanied with the increase in particle diameter and with the ordering of the FePt superlattice. The critical diameter for emergence of ferromagnetism of FePt particle has been considered to be 3.6 to 5.6 nm in mean diameter, under the existence of the ordered L10 phase The blocking temperature as a function of the annealing temperature was investigated
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Key engineering materials Vol. 319 (Sept. 2006), p. 39-44 
    ISSN: 1013-9826
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Effects of hydrogen doping on the internal friction (IF) of ternary Ti50Ni50-xCux (x=15, 20,25)[removed info] shape memory alloys, prepared by rolling and annealing laminating Ti and Ni-Cu alloy sheets,have been measured with a damping mechanical analyzer in a forced bending oscillation mode attemperatures from 173K to 423K at three frequencies, 0.1, 1 and 5Hz. The effects of hydrogendoping on IF are common to the three alloys: a hydrogen IF peak appears at around 260K; the IFpeak value (tanφ) increases rapidly with increasing hydrogen concentration up to tanφ=0.03 at0.5at% and then decreases; the peak temperature also increases rapidly and then gradually decreases.From the frequency dependence of the peak temperature, the activation energy E and thepre-exponential factor ω0 have been analyzed to be E=0.6-0.7eV and ω0=1013-14s-1. The origin of thehydrogen IF is interpreted to be the Snoek-Koester effect due to interaction of twin boundarydislocations and segregated hydrogen atoms. Effects of hydrogen on mechanical properties of thealloys have also been studied
    Type of Medium: Electronic Resource
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  • 3
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Key engineering materials Vol. 319 (Sept. 2006), p. 67-72 
    ISSN: 1013-9826
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: M2052 alloy is a MnCu based high damping alloy that shows high damping capacity andthe superior workability. In the present work, the microstructure and damping behavior of the alloy indifferent solidification cooling rates are investigated with directionally cast alloy plate. For thevariation of solidification cooling rate in the range of 250~10K/s, the secondary dendrite arm spacingof the cast alloy changes from 4 to 18mm and grain size varies in the range of 100~200mm except thesurface regions and center regions in the cast plate. As compared to the worked and heat treated alloy,the as-cast alloy shows a high temperature damping above the average phase transformationtemperature of the alloy irrespective to the solidification cooling rate. On the other hand, a higherdamping peak is observed in the cast alloy which is attributed much to the twin boundary damping,however, the magnitudes of the damping peak are found to be varied corresponding to the respectivesolidification conditions
    Type of Medium: Electronic Resource
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