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  • Electronic Resource  (5)
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  • Electronic Resource  (5)
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  • 1
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Materials science forum Vol. 475-479 (Jan. 2005), p. 3149-3152 
    ISSN: 1662-9752
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: A Monte Carlo Potts model has been used to investigate cube-texture strengthening during grain growth in rolled high-purity Ni-tapes. The initial conditions for the simulations have been taken from electron back-scatter pattern (EBSP) orientation maps of already fully recrystallized samples. Experimentally, grain growth leads to an increase in the cube volume fraction to 〉95% , accompanied by an approximately ten-fold increase in the grain size. High cube volume fractions can be predicted under a number of conditions, though a small surface energy advantage of just 2% for cube-oriented grains is required to match the texture strengthening to the grain size change. An additional issue of interest is the influence on the grain growth of the large area-fraction of twin boundaries in the fully recrystallized condition. The presence of boundaries with low energy has a strong influence on thesimulated microstructural evolution
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Materials science forum Vol. 495-497 (Sept. 2005), p. 231-236 
    ISSN: 1662-9752
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: The effect of orientation noise in EBSP data on measurement of percolation thresholdvalues has been investigated by use of computer simulated microstructures. A 2-D Monte Carlo Potts model run on a square lattice of size 200 x 200 was used to generate a microstructure containing approximately 150 grains. Orientations were then assigned to each of these grains to generate single texture component microstructures of differing texture tightness (“model” data). In order to simulatethe effect of orientation noise on the experimental data, the orientation at each point in the 200 x 200 grid was adjusted in a manner consistent with experimental observations of the effect of orientation noise. The model data represent therefore an underlying real grain structure, and the noise-adjusted data represent the orientation map that would be measured using EBSP analysis at a given orientationnoise level. The misorientation angle q70% at which 70% of the grains were percolatively connected was then determined for both the ideal data and for the orientation noise adjusted data. A comparison of the two allows calibration of the extent to which percolation data may be incorrectly estimated by EBSP measurements
    Type of Medium: Electronic Resource
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  • 3
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Materials science forum Vol. 495-497 (Sept. 2005), p. 1467-1474 
    ISSN: 1662-9752
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: In this paper we report a study using fully automated EBSP orientation measurements onthe texture and microstructure of fully processed Bi-2223 tapes produced by the powder-in-tubemethod. For the automated analysis a new unit cell describing the quasi-tetragonal Bi-2223 phase hasbeen developed. The texture data confirm that a strong fibre texture is produced during processing,with the c-axis of the Bi2223 plates parallel to the tape normal direction. Quantitative analysissuggests that the orientation density along the fibre texture is close to random. In contrast the distribution of misorientations shows significant correlations between the orientations, and is skewed towards low misorientation angles. A more detailed investigation reveals that the structure consists of colonies of plates, with low angle misorientations within each colony. Analysis of the rotation axes shows some differences as a function of misorientation angle
    Type of Medium: Electronic Resource
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  • 4
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Materials science forum Vol. 495-497 (Sept. 2005), p. 1309-1314 
    ISSN: 1662-9752
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Ni with columnar grain was cold rolled and then recrystallized. The orientations at triple junctions before and after annealing were characterised using the EBSD technique, and recrystallization nuclei at triple junctions were identified. A comparison was made between the orientations of the nuclei and the orientations of the grains in the same area before annealing. Both nuclei with orientations within the orientation spread of the deformed grains as well as away from that were found
    Type of Medium: Electronic Resource
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  • 5
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Materials science forum Vol. 495-497 (Sept. 2005), p. 1315-1322 
    ISSN: 1662-9752
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: A 10 Tesla magnetic field was applied during annealing of cold-rolled high purity Ni at300°C for 2 hours, with samples aligned at various different angles to the magnetic field direction. The effect of the magnetic field annealing on the cube texture evolution and the microstructural development was investigated by use of electron backscatter pattern (EBSP) analysis in the scanning electron microscope. The results show that both the cube texture evolution and the grain size are affected by the application during annealing of a high strength magnetic field, and that the effect varies as a function of the angle between the sample normal and the magnetic field direction. The cube texture volume fraction resulting from 2 hours annealing increases with increasing angle between the field direction and the sample normal direction, though in nearly all cases lower cube volume fractions were obtained compared to annealing without a magnetic field. The average size for all grains and for just cube-oriented grains both decrease with decreasing cube texture fraction, suggesting that the presence of a magnetic field either leads to enhanced recrystallization nucleation, or to a retardation of grain growth after recrystallization
    Type of Medium: Electronic Resource
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