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Synthesen in der Isocamphanreihe, 39. Mitt.: Verbesserung derDiels-Alder-Reaktion von Cyclopentadien mit Mesityloxid durch Ultraschall und eine neue Synthese von Dehydrocamphen (1994)

Buchbauer, G. ; Spreitzer, H. ; Bauer, I. ; [et al.]

Springer

Monatshefte für Chemie 125 (1994), S. 921-925

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ISSN: 1434-4475

Keywords: 2-Acetyl-3,3-dimethylbicyclo[2.2.1]hept-5-ene ; Camphene ; 5,5-Dimethyl-6-methylenebicyclo[2.2.1]hept-2-ene ; Isocamphane derivatives ; Isocamphodiene ; Norborn-5-ene derivatives ; Odour ; Sonification ; Ultrasound chemistry

Source: Springer Online Journal Archives 1860-2000

Topics: Chemistry and Pharmacology

Notes: Summary The synthesis of the valuable terpenic synthon 2-acetyl-3,3-dimethylbicyclo[2.2.1]hept-5-ene is clearly improved concerning the yield and especially the reaction time by applying ultrasound on theDiels-Alder reaction of cyclopentadiene with mesityl oxide. A new synthesis of dehydrocamphene and its odour impression is described.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1007/BF00812706

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