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A NMR method to probe the nature of liquid clathrates (1986)

Barden, Laura M. ; Babaian, Elizabeth A. ; Sherry, A. Dean ; [et al.]

Springer

Journal of inclusion phenomena and macrocyclic chemistry 4 (1986), S. 429-431

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ISSN: 1573-1111

Keywords: Liquid clathrate ; NMR ; aluminium alkyl

Source: Springer Online Journal Archives 1860-2000

Topics: Chemistry and Pharmacology

Notes: Abstract The liquid clathrate formed from [N(CH3)4][Al2(CH3)6I] and benzene has been studied using 200 MHz1H FT-NMR. Two resonances, corresponding to the free and guest benzene are observed. The1H spin lattice relaxation times,T 1, for these molecules were measured and found to be distinctly different. The guest benzene protons relax nearly four times faster than the free molecules which is consistent with a more ordered structure of the benzene molecules within the clathrate.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1007/BF00656170

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