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Digitale Medien

Determination of amino acids by gas chromatography using a wide bore capillary column (1987)

Moodie, I. M. ; Burger, J. A. ; Labadarios, D.

Weinheim : Wiley-Blackwell

Journal of High Resolution Chromatography 10 (1987), S. 383-387

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Details

ISSN: 0935-6304

Schlagwort(e): Gas chromatography ; Wide bore glass capillary ; Fused-silica capillary ; Component discrimination ; Butt connectors ; Chemistry ; Analytical Chemistry and Spectroscopy

Quelle: Wiley InterScience Backfile Collection 1832-2000

Thema: Chemie und Pharmazie

Notizen: A procedure is described in which a wide bore capillary column is used as an alternative to the more traditional packed column for the quantitative analysis of amino acids as their N-heptafluorobutyryl isobutyl ester (HBB) derivatives. The column, installed in a gas chromatograph previously configured for use with a packed column, is shown to give good reproducibility by repeated determination of amino acid response factors (RSD values for all amino acids are below 3%). A number of problems, encountered during the use of this column, are discussed and suitable techniques to overcome them are reported.

Zusätzliches Material: 4 Ill.

Materialart: Digitale Medien

URL: http://dx.doi.org/10.1002/jhrc.1240100703

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