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Deactivation, coating and performance of nickel capillary columns for GLC (1986)

Rohwer, E. R. ; Pretorius, V. ; Hulse, G. A.

Weinheim : Wiley-Blackwell

Journal of High Resolution Chromatography 9 (1986), S. 30-34

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ISSN: 0935-6304

Keywords: Gas chromatography, GC ; Nickel capillary columns ; Chemistry ; Analytical Chemistry and Spectroscopy

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: Electroformed nickel tubing was deactivated by chemical vapor deposition of silicon from silane gas and subsequent treatment with cyclooctamethyltetrasiloxane (D4). Standard activity tests performed on the uncoated tube and also on columns coated with crosslinked and uncrosslinked, nonpolar stationary phase, show that good quality flexible columns can be prepared from nickel tubing. The inner surface of the silicon coated tube was characterized by Auger depth profile analysis.

Additional Material: 6 Ill.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/jhrc.1240090105

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