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An improved gas chromatographic assay for spectinomycin hydrochloride (1994)

Hoebus, J. ; Yun, Li Ming ; Hoogmartens, J.

Springer

Chromatographia 39 (1994), S. 71-73

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ISSN: 1612-1112

Keywords: Gas chromatography ; Spectinomycin ; Silylation

Source: Springer Online Journal Archives 1860-2000

Topics: Chemistry and Pharmacology

Notes: Summary A gas chromatographic assay for spectinomycin hydrochloride is described. The method is based on that prescribed by the United States Pharmacopeia (USP XXII). The method involves silylation of spectinomycin hydrochloride; phenazone is used as an internal standard. Spectinomycin and phenazone have adequate stability under the prescribed conditions. The stationary phase is 3% OV-17 on Gaschrom Q 100–120 mesh. The selectivity of the proposed method is better than that of the GLC method described in the USP XXII.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1007/BF02320461

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