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Origins of phase anomalies in 13C FT NMR spectra (1987)

Anet, Frank A. L. ; Zheng, Li Kao ; Zhihong, Tan

Chichester : Wiley-Blackwell

Organic Magnetic Resonance 25 (1987), S. 439-442

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ISSN: 0749-1581

Keywords: 13C NMR ; Phase anomalies ; Echoes Sampling effects ; Chemistry ; Analytical Chemistry and Spectroscopy

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: Some controversy exists on the origin(s) of phase anomalies observed in 13C FT NMR spectra. Two separate explanations, based on either echo or sampling effects, have been proposed by previous workers. We now show experimentally that these two effects can occur separately or together and, in the latter case, the effects can interfere with one another. Methods to ameliorate or remove phase anomalies are briefly reviewed.

Additional Material: 2 Ill.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/mrc.1260250511

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