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Digitale Medien

Use of non-segmented flow, post-columns reaction detection with miniaturized HPLC systems (1983)

Apffel, J. A. ; Brinkman, U. A. Th. ; Frei, R. W.

Springer

Chromatographia 17 (1983), S. 125-131

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Details

ISSN: 1612-1112

Schlagwort(e): Miniaturized HPLC ; Post-column reaction detection ; Catecholamines ; Packed-bed reactors ; Non-segmented open-tubular reactors

Quelle: Springer Online Journal Archives 1860-2000

Thema: Chemie und Pharmazie

Notizen: Summary The use of non-segmented flow, post-column reaction detection is evaluated for use with miniaturized HPLC. Non-segmented open-tubular reactors with internal diameters 0.1 mm to 0.25 mm and packed-bed reactors with internal diameters of 1 mm, filled with 5 and 10 μm particles are evaluated theoretically and experimentally with respect to band broadening and pressure drop characteristics. An integrated system consisting of miniaturized HPLC (1 mm i. d.) columns and compatible hardware is described. An example of the separation of catecholamines is given.

Materialart: Digitale Medien

URL: http://dx.doi.org/10.1007/BF02271034

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