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Reinvestigation of the structure of 1:3,2:4,5:6-tri-O-isopropylidene-D-glucitol by 1H NMR spectroscopy at 250 MHz (1983)

Sohár, P. ; Kuszmann, J.

Chichester : Wiley-Blackwell

Organic Magnetic Resonance 21 (1983), S. 694-697

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ISSN: 0030-4921

Keywords: Chemistry ; Analytical Chemistry and Spectroscopy

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: The structure of 1:3,2:4,5:6-tri-O-isopropylidene-D-glucitol, which was proposed earlier to be the 1:2,3:5,4:6-analogue, was re-detormined by 1H NMR measurement at 250 MHz. The assignments were proved by double resonance experiments. Using the spectral parameters as starting values, the theoretical spectrum of the eight skeletal protons was constructed and the chemical shifts and proton-proton coupling constants were calculated by iteration (RMS: 0.014) using the PANIC program of Bruker AG.

Additional Material: 2 Ill.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/omr.1270211112

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