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Smoothing and validity of crystallite-size distributions from X-ray line-profile analysis (1978)

Le Bail, A. ; Louër, D.

Copenhagen : International Union of Crystallography (IUCr)

Applied crystallography online 11 (1978), S. 50-55

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Details

ISSN: 1600-5767

Quelle: Crystallography Journals Online : IUCR Backfile Archive 1948-2001

Thema: Geologie und Paläontologie , Physik

Notizen: A smoothing procedure is described which eliminates spurious details on crystallite-size distribution functions deduced from X-ray line profiles. It is based on a least-squares process with a stabilization scheme and is applied to composite specimens prepared by mixing known quantities of samples of nickel hydroxide, whose crystallite size-distribution functions were previously determined. Calculated and observed distributions and average sizes are compared. The results are reasonably good and show the self-consistency of the method.

Materialart: Digitale Medien

URL: http://dx.doi.org/10.1107/S0021889878012662

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