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Preparation of 1,2=dialkylcycloalkanes synthesisis of the stereoisomeric 1-butyl-2-methylcyclopentanes (1953)

Plate, A. F. ; Liberman, A. L. ; Momma, N. A.

Springer

Russian chemical bulletin 2 (1953), S. 617-623

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Details

ISSN: 1573-9171

Quelle: Springer Online Journal Archives 1860-2000

Thema: Chemie und Pharmazie

Notizen: Summary 1. A suitable p~reparative method has been proposed for obtaining 2-methylcyclopentanone: it consists in the dehydration of the diol obtained b y oxidizing 1-methylcyclopentene with a mixture of hydrogen peroxide and formic acid. 2. It has been shown that this method is of no value for the preparation of 2-methylcyclohexanone: in the case of the six-membered cycle, dehydration of the diol is accompanied by isomerization side reaction. 3. 1-Butyl-2-methyleyclopentane has been synthesized from 2-methylcyclopentanone prepared by the above method, and it has been separated into its cis and trans isomers.

Materialart: Digitale Medien

URL: http://dx.doi.org/10.1007/BF01171783

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