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  • 1
    ISSN: 1573-1561
    Schlagwort(e): (9z,11Z) ; (9E.11E) ; (9E,11Z) ; (9Z,11E)-9 ; 11-Hexadecadienals ; (9E)-hexadecen-11-yn-1-yl acetate ; syntheses ; aldehydes ; ester ; conjugated dienes ; dienals
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Biologie , Chemie und Pharmazie
    Notizen: Abstract The title compounds were prepared by six different routes, and recommendations are given for the more convenient procedures in laboratory-scale syntheses. Modifications in the literature preparations of the 9E,11E and 9E,11Z isomers are described. Baseline separation of a prepared mixture of all four isomers of the (9Z, 11Z), (9E, 11E), (9E, 11Z), and (9Z, 11E)-9,11-hexadecadienals was achieved using GC methods with standard capillary columns. [13C]NMR spectroscopy of the alkene carbon atoms clearly differentiates between theZ,Z, E,E and eitherE,Z orZ,E isomers of the precursor dienols and thus of the dienals.
    Materialart: Digitale Medien
    Bibliothek Standort Signatur Band/Heft/Jahr Verfügbarkeit
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  • 2
    Digitale Medien
    Digitale Medien
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 35 (1992), S. 391-408 
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: A six noded triangular finite element has been proposed to model variable order singularities in the first derivatives of field variables occurring at multiple locations (up to three) lying in close proximity. The element satisfies the convergence requirements fully. The element will be very useful in the analysis of neighbouring cracks, zig-zag cracks, kinked cracks, etc., involving mechanical and/or thermal loadings. The first degenerate form, which is a two point variable order singularity element, can be used, for example, to cover the distance between two adjacent crack tips. The second degenerate form, which is a one point variable order singularity element, can be used around a crack tip like any other crack tip elements. Six case studies have been reported, three involving mechanical loadings and the other three thermal loadings. These have helped to check the performance of the element and its two degenerate forms. The accuracy of the results in all the examples is good.
    Zusätzliches Material: 10 Ill.
    Materialart: Digitale Medien
    Bibliothek Standort Signatur Band/Heft/Jahr Verfügbarkeit
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  • 3
    Digitale Medien
    Digitale Medien
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 33 (1992), S. 1955-1974 
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: An element for analysis of variable order one point singularities in plane problems has been proposed. The element meets all the convergence requirements, viz. the rigid body mode, the constant strain condition and the interelement compatibility. It can be easily incorporated in any package based on the displacement formulation. Four examples from fracture mechanics are presented to demonstrate its performance. The examples involve mechanical or thermal loadings. The accuracy of results in all the examples is very good.
    Zusätzliches Material: 9 Ill.
    Materialart: Digitale Medien
    Bibliothek Standort Signatur Band/Heft/Jahr Verfügbarkeit
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  • 4
    Digitale Medien
    Digitale Medien
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 28 (1989), S. 1449-1460 
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: An element formulation is suggested to obtain variable order singularities simultaneously at the two neighbouring corner nodes of a 4-noded quadrilateral. The element is useful for modelling a kinked crack with small kink length. The accuracy is good and this is obtained at a substantially reduced computational cost. Case studies are presented to illustrate the usefulness and the accuracy obtainable.
    Zusätzliches Material: 6 Ill.
    Materialart: Digitale Medien
    Bibliothek Standort Signatur Band/Heft/Jahr Verfügbarkeit
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  • 5
    Digitale Medien
    Digitale Medien
    Chichester [u.a.] : Wiley-Blackwell
    International Journal for Numerical Methods in Engineering 29 (1990), S. 1487-1499 
    ISSN: 0029-5981
    Schlagwort(e): Engineering ; Engineering General
    Quelle: Wiley InterScience Backfile Collection 1832-2000
    Thema: Mathematik , Technik allgemein
    Notizen: A 3-noded triangular two singular points finite element is proposed to model two variable order singularities lying at close proximities as in the case of a kinked crack. The element meets the rigid body mode and the interelement compatibility of the convergence criteria. A degenerate form of the element is a one point variable order singularity element, which meets all the convergence requirements. A number of kinked crack problems have been analysed using the new element and its degenerate form. The computed results are compared with analytical solutions. The accuracy of the results is found to be good.
    Zusätzliches Material: 9 Ill.
    Materialart: Digitale Medien
    Bibliothek Standort Signatur Band/Heft/Jahr Verfügbarkeit
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