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  • 1-Benzyl-6-phenylpiperidin-2-one-5-carboxylic acid  (1)
  • aluminium determination  (1)
  • crack tip opening displacement CTOD  (1)
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Years
Keywords
  • 1
    Electronic Resource
    Electronic Resource
    Springer
    Acta mechanica solida Sinica 3 (1990), S. 263-276 
    ISSN: 0894-9166
    Keywords: elastic-plastic fracture ; three dimensional stress field ; transition layer ; crack tip opening displacement CTOD
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract In this paper, the stress and strain structures of Mode I 3-D crack in power hardening material are studied by analyzing the fundamental equations of elastic-plastic mechanics. It is shown that three regions, Z1,Z2 and Z3 can be divided in the thickness direction according to the stress characteristic. In region Z1, the stress components in the plane Perpendicular to z axis (thickness direction) can be solved first using the fundamental equations of plane strain state; in region Z3, they can be solved first by the equations of plane stress state. The region Z2 is defined as a transition layer. It is shown that the transition layer is the characteristic of Mode I 3-D crack in elastic-plastic state, and it is significant to the research on 3-D fracture. The crack tip opening displacement CTOD is chosen to describe the amplitude coefficient of the local stress field, and the distribution of CTOD in 3-D state is investigated.
    Type of Medium: Electronic Resource
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  • 2
    ISSN: 1573-1111
    Keywords: 1-Benzyl-6-phenylpiperidin-2-one-5-carboxylic acid ; acetonitrile ; inclusion compound ; hydrogen bonding ; disorder
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Abstract C19H19NO3·x CH3CN (x=0.3),M r=643.35, hexagonal, space groupP61 (No. 169),a=23.027(5),c=5.775(1) Å,V=2652(1) Å3,Z=6. The structure was solved by direct methods and refined toR=0.077 for 1562 observed MoK α reflections. The title heterocyclic carboxylic acid was established as thetrans isomer, with the phenyl and carboxyl substituents occupying pseudo-equatorial and equatorial positions, respectively, of the piperidin-2-one ring in a half-chair conformation. Acid host molecules related by the 61 screw operation are linked by intermolecular O−H...O (cyclic amide) hydrogen bonds to generate an open channel bounded by coaxial intertwined helices each having a pitch of 5c. Within each channel of free diameterca. 6.0 Å the acetonitrile molecules partially occupy highly disordered sites which do not lie on thec axis.
    Type of Medium: Electronic Resource
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  • 3
    Electronic Resource
    Electronic Resource
    Springer
    Microchimica acta 100 (1990), S. 299-304 
    ISSN: 1436-5073
    Keywords: bio-membrane ; fibre optic sensor ; immobilized morin ; aluminium determination
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Abstract A new type of fibre optic sensor based on the use of bio-membrane is proposed for the determination of aluminium. Morin is immobilized on mutton membrane pre-treated with formaldehyde and attached to the fibre optic. Fluorescence response is linear from 8 × 10−7 to 3 × 10−5M. The detection limit is 6 × 10−7 M. Response time is 30—60 s.
    Type of Medium: Electronic Resource
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