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  • 1
    Electronic Resource
    Electronic Resource
    Springer
    Journal of sol gel science and technology 8 (1997), S. 391-395 
    ISSN: 1573-4846
    Keywords: silica xerogels ; crystallization ; Raman spectroscopy ; Eu3+ luminescence
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Abstract Pure and europium doped silica xerogels were annealed at 1050°C to obtain full densification, and at 1300°C to induce crystallization. Raman spectroscopy, time resolved selective luminescence and lifetime measurements were performed on glassy and crystallized samples. We discuss the differences between the Raman spectra of the xerogel annealed at 1050°C and those of a commercial silica. The typical Raman structures of α -crystobalite are evident for the 1300°C annealed samples, but a glassy phase coexists, indicating an incomplete crystallization. Fluorescence measurements give information on the environment of the Eu3+ ions in the glassy and crystallized sample.
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    Springer
    Journal of sol gel science and technology 8 (1997), S. 391-395 
    ISSN: 1573-4846
    Keywords: silica xerogels ; crystallization ; Raman spectroscopy ; Eu3+ luminescence
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Abstract Pure and europium doped silica xerogels were annealed at 1050°C to obtain full densification, and at 1300°C to induce crystallization. Raman spectroscopy, time resolved selective luminescence and lifetime measurements were performed on glassy and crystallized samples. We discuss the differences between the Raman spectra of the xerogel annealed at 1050°C and those of a commerical silica. The typical Raman structures of α-crystobalite are evident for the 1300°C annealed samples, but a glassy phase coexists, indicating an incomplete crystallization. Fluorescence measurements give information on the environment of the Eu3+ ions in the glassy and crystallized sample.
    Type of Medium: Electronic Resource
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  • 3
    Electronic Resource
    Electronic Resource
    Springer
    European journal of epidemiology 1 (1985), S. 274-280 
    ISSN: 1573-7284
    Keywords: Rotavirus ; Bovine ; Simian ; Porcine
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Notes: Abstract Three rotavirus strains of bovine, simian and porcine origin, respectively, were compared. The 3 viruses induced a classic rotavirul infection in newborn, conventionally reared calves. The cross neutralization tests revealed an antigenic identity of simian and porcine rotaviruses and a slight serologic correlation of these two viruses with the bovine rotavirus strain. However, in reciprocal cross protection tests carried out in calves, the simian rotavirus antiserum afforded weak protection to challenge infection with either the porcine or the bovine viruses. By contrast, the protective level of the bovine and the porcine rotavirus antisera was relatively high. It was speculated that the 81/36F bovine rotavirus could be considered, tentatively, as an antigenic reassortant rotavirus strain.
    Type of Medium: Electronic Resource
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  • 4
    Electronic Resource
    Electronic Resource
    Springer
    European journal of epidemiology 5 (1989), S. 279-284 
    ISSN: 1573-7284
    Keywords: Rotavirus ; Immunization ; Calves
    Source: Springer Online Journal Archives 1860-2000
    Topics: Medicine
    Notes: Abstract Calves fed with colostrum from cows vaccinated with an inactivated rotavirus vaccine were refractory to experimental infection with strain 81/36F of bovine rotavirus. In the field study, 458 pregnant cows from 26 herds were involved. In each herd, cows were selected and randomly subdivided in two groups. Cows in one group (248 head in total) were vaccinated, whereas cows in the other group (210 head in total) were left as unvaccinated controls. At calving, colostrum was collected from each cow and stored at -30°C until used for feeding calves. The newborn calves, beginning the second day of life and for the next 740 days, were each fed a daily supplement of 400 ml of colostrum from its dam. The diarrhea occurred in 86 (40.9%) calves that had received colostrum from unvaccinated dams (normal colostrum), and in 7 (2.8%) calves which were fed colostrum from vaccinated dams (immune colostrum). The disease was very severe in the normal colostrum-fed calves and 52 of them died. By contrast, the 7 immune colostrum-fed calves displayed a rather mild enteric condition, and all recovered without any sequela being observed.
    Type of Medium: Electronic Resource
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  • 5
    Electronic Resource
    Electronic Resource
    Chichester : Wiley-Blackwell
    Organic Magnetic Resonance 33 (1995), S. 657-663 
    ISSN: 0749-1581
    Keywords: NMR ; 1H NMR ; 13C NMR ; dimers and timers of 3-hexylthiophene ; poly(3-hexylthiophene) ; 1H, 13C inverse detection ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: The 1H and 13C signals of the hexyl chains of the title compounds were fully assigned. The regiochemical features of the aliphatic region of proton and carbon spectra were analysed in dimers and trimers. Dimers and trimers proved to be reliable model compounds in the regiochemical assignment of poly(3-hexylthiophene) even when the aliphatic region of proton and carbon spectra was involved. The chemical shifts of the protons of CH2(α)s and of the hexyl chain as a whole and those of the first three aliphatic carbons appear to be the most significant.
    Additional Material: 5 Ill.
    Type of Medium: Electronic Resource
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