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  • 1
    Electronic Resource
    Electronic Resource
    Fluorescence-excitation and hole-burning spectroscopy of heavy-dose neutron-irradiated α-Al2O3 (1995)
    Springer
    Applied physics 60 (1995), S. 507-512 
    Details
    ISSN: 1432-0649
    Keywords: 42.70 ; 81.40 ; 61.80
    Source: Springer Online Journal Archives 1860-2000
    Topics: Physics
    Notes: Abstract We report on persistent spectral hole-burning and fluorescence-excitation spectroscopy in heavy-dose (3 × 1020 n/cm2) neutron-irradiated and annealed sapphire using a Ti:Sapphire ring laser in single-frequency and broad-band operation. The optimum conditions for hole burning were obtained after annealing the crystals to 400 °C. Holes have been detected in the near-infrared spectral range between 745 and 795 nm. At 1.5 K, the narrowest hole widths were approximately 2 GHz, so that about 104 holes can be burnt in this spectral region. Besides the storage density in the wavelength dimension, the coefficient describing the electric-field-induced filling of a spectral hole also rises by more than one order of magnitude as compared to crystals with low neutron-irradiation dose.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1007/BF01080928
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    Paper (German National Licenses)
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  • 2
    Electronic Resource
    Electronic Resource
    1H NMR and molecular mechanics studies of epimeric ethyl esters of 20(R, S)-hydroxy-23-norcholanoic acids (1991)
    Chichester : Wiley-Blackwell
    Organic Magnetic Resonance 29 (1991), S. 137-142 
    Details
    ISSN: 0749-1581
    Keywords: 20(R,S)-Hydroxy-23-norcholanoic acid derivatives ; 1H NMR ; Pyridine-induced shifts ; Molecular mechanics calculations ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Proton chemical shifts for the C-18, C-21, —CO2CH2CH3 and —CO2CH2CH3 protons of epimeric ethyl esters of 20(R,S)-hydroxy-23-norcholanoic acids were measured in deuteriochloroform and pyridine-d5. The observed solvent shifts due to specific OH - pyridine hydrogen-bonded complexes allowed the quantification of the epimeric mixtures by analysis of the pyridine-d5 1H NMR spectra. The main features of the pyridine-induced shifts are rationalized in terms of the preferred conformations for the 20R- and 20S-epimers, which are predicted by molecular mechanics calculations.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/mrc.1260290208
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    Paper (German National Licenses)
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