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1H and 13C NMR assignments of the antitumor macrolide bryostatin 1 (1991)

Schaufelberger, Daniel E. ; Chmurny, Gwendolyn N. ; Koleck, Mary P.

Chichester : Wiley-Blackwell

Organic Magnetic Resonance 29 (1991), S. 366-374

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ISSN: 0749-1581

Keywords: Bryostatin 1 ; NMR data ; Structure ; Chemistry ; Analytical Chemistry and Spectroscopy

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: During a large-scale isolation of bryostatin 1, NMR measurements indicated that parts of the published 13C and 1H NMR assignments had to be revised. These reassignments were based on extensive homonuclear and heteronuclear one- and two-dimensional NMR techniques performed at 500 MHz. These independently obtained assignments are also in good agreement with the revised assignments and structure of bryostatin 3.

Additional Material: 5 Ill.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/mrc.1260290414

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