ISSN:
0935-6304
Keywords:
Gas chromatography
;
Capillary, glass
;
Sample preparation by pre-chromatographic reaction at the 7 microliter level
;
Reproducibility of methylation and allylation of barbiturates
;
Application to blood analysis
;
Chemistry
;
Analytical Chemistry and Spectroscopy
Source:
Wiley InterScience Backfile Collection 1832-2000
Topics:
Chemistry and Pharmacology
Notes:
Pre-chromatographic reactions are no longer a necessary evil. Equipment such as the microrefluxer now allows reproducible 7-μl-reactions to be carried out in a short time. Thus multiple derivatisations can be used together with glass capillary GC for routine identifications. The method has been succesfully applied to barbiturates. Retention data of their methyl-, allyl- and benzyl-derivatives are given.Quantitative blood level determinations are briefly discussed.
Additional Material:
6 Ill.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1002/jhrc.1240020619
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