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  • Chemical Engineering  (2)
  • Creatinine deiminase  (1)
  • Herbal medicines  (1)
  • 1
    Electronic Resource
    Electronic Resource
    Amsterdam : Elsevier
    Clinica Chimica Acta 185 (1989), S. 241-252 
    ISSN: 0009-8981
    Keywords: Creatinine analysis ; Creatinine deiminase ; Enzymatic analysis ; N-Carbamoylsarcosine amidohydrolase ; N-Methylhydantoin amidohydrolase
    Source: Elsevier Journal Backfiles on ScienceDirect 1907 - 2002
    Topics: Medicine
    Type of Medium: Electronic Resource
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  • 2
    ISSN: 1612-1112
    Keywords: Gas chromatography-mass spectrometry ; Organochlorine and organophosphorus pesticides ; Herbal medicines ; Selective-ion monitoring
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Summary Multicomponent pesticide residues in herbal medicines have been analyzed by gas chromatography-mass spectrometry (GC-MS) with electron impact (EI) ionization and positive- and negative-ion chemical ionization (PCI and NCI). Herbal medicines (5 g) were extracted with 65∶35 (%,v/v) acetonitrile-water, and partitioned with hexane-diethyl ether (1∶1) and hexane-dichloromethane (1∶1). The organic phase of the extracted fraction was cleaned on a Florisil column and analyzed by GC-MS with selected-ion monitoring (SIM). Method detection limits for 27 pesticides were tens of picograms for ECD, NPD and EI-SIM MS, and a few picograms for NCI-SIM MS. The calibration curve for the pesticide standard solution was linear within the range 0.003–30 pg for EI-SIM MS, PCI-SIM MS, and NCI-SIM MS. Mean recoveries of pesticides from spiked herbal medicines (0.75, 1.5, 3 pg) were 61–125% (RSD1–32%) for NCI-SIM MS and 74–121% (RSD 4–12%) for EI-SIM MS. Detection sensitivity and specificity of NCI-SIM MS were better than for ECD and NPD. Parallel use of EI-SIM MS, PCI-SIM MS and NCI-SIM MS was an excellent complementary method for identification and confirmation of multi-component pesticide residues in variety of herbal medicines.
    Type of Medium: Electronic Resource
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  • 3
    Electronic Resource
    Electronic Resource
    Hoboken, NJ : Wiley-Blackwell
    AIChE Journal 29 (1983), S. 353-360 
    ISSN: 0001-1541
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Process Engineering, Biotechnology, Nutrition Technology
    Notes: Pressure drop for a gas-solids suspension flowing concurrently downward in a 13-mm inside-diameter tube was investigated using 329-micron spherical glass beads in air. The gas Reynolds number varied from 0 to 30,000 with solids-loading ratios of up to 20 at a gas Reynolds number of 10,000. The frictional pressure drop for downflow was found to be a weaker function of the solids-loading ratio than the upflow case using data reported in the literature. Empirical correlation of the two-phase friction factor, in terms of the gas Reynolds number and a dimensionless parameter, CDEPD/[(1 - Ep)dp], showed that at high solids loadings, particles tend to stabilize the suspension flow. The dimensionless parameter seems to be applicable to a universal pressure drop correlation for solids-fluid systems, but requires further investigation.
    Additional Material: 13 Ill.
    Type of Medium: Electronic Resource
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  • 4
    Electronic Resource
    Electronic Resource
    Hoboken, NJ : Wiley-Blackwell
    AIChE Journal 29 (1983), S. 306-312 
    ISSN: 0001-1541
    Keywords: Chemistry ; Chemical Engineering
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Process Engineering, Biotechnology, Nutrition Technology
    Notes: Heat transfer to a gas-solids suspension flowing cocurrently downward in a 13-mm inside diameter tube with uniform heat-flux boundary conditions was investigated using 329-μm spherical glass beads in air. The gas Reynolds number varied from 0 to 30,000 with solids-loading ratios of up to 20 at a gas Reynolds number of 10,000. The suspension Nusselt number, defined in terms of the wall-to-gas mixed-mean temperature difference, decreased with increasing solids-loading ratio at high Reynolds numbers, while it changed little from the value for gas alone at low Reynolds numbers. A possible explanation is given by considering the effects of particles on the fluid mechanical properties of the gas. Asymptotic Nusselt numbers in downflow are compared with results of other investigations for upflow.
    Additional Material: 12 Ill.
    Type of Medium: Electronic Resource
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