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  • Chemistry  (6)
  • 1
    Electronic Resource
    Electronic Resource
    A new selective agent for poly(tetrahydrofuran) degradation as a tool for the determination of the crystallite core size (1991)
    New York : Wiley-Blackwell
    Die Makromolekulare Chemie 192 (1991), S. 1177-1181 
    Details
    ISSN: 0025-116X
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Notes: The method formerly used to determine the crystallite core size of polyethylene was applied to poly(tetrahydrofuran) (PTHF). This method is based on the different diffusivity of a chaincleaving agent in crystalline and amorphous parts of the polymer. Butyllithium was used as a cleaving agent of PTHF. The degree of polymerization of the undecomposed part of the polymer (PTHF crystallites) was determined by gel permeation chromatography. This value agrees well with the value to be expected from the size of the crystallites determined small-angle X-ray scattering.
    Additional Material: 5 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/macp.1991.021920516
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    Paper (German National Licenses)
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  • 2
    Electronic Resource
    Electronic Resource
    Synthesis of poly(N-vinylcarbazole)-graft-polyisoprene (1995)
    Weinheim : Wiley-Blackwell
    Macromolecular Chemistry and Physics 196 (1995), S. 485-489 
    Details
    ISSN: 1022-1352
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Physics
    Notes: Well defined poly(N-vinylcarbazole)-graft-polyisoprenes were synthesized by reaction between the chloromethyl group of chloromethylated poly(N-vinylcarbazole) and living polyisoprene (PIP) anions. The obtained graft copolymers were characterized by gel-permeation chromatography, NMR, and IR spectra. The reaction was not complete (unreacted chloromethyl groups were found) because of hindrance effects of the polyisoprene chain.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/macp.1995.021960204
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    Paper (German National Licenses)
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  • 3
    Electronic Resource
    Electronic Resource
    Observation technique of polymer micelle by using transmission electron microscope (1990)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 40 (1990), S. 1547-1555 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: The method, established by Price et al. to observe the polymer micelle, was modified and applied to the region of high polymer concentration. The novelty of our method consists of the preparative method of the specimen for transmission electron microscopy. Polymer solution was diluted and solvent was evaporated rapidly before the micelle was decomposed. As a result, dilution ratio had no effect on the decomposition of polymer micelle, and the original micelle structure was conserved over 10 wt % block copolymer solution if the operations were carried out within 30 min. This time limit related to the concentration of solution.
    Additional Material: 8 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1990.070400912
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    Paper (German National Licenses)
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  • 4
    Electronic Resource
    Electronic Resource
    Morphologies of poly(vinylcarbazole)-polyisoprene graft copolymer and blend (1995)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 55 (1995), S. 125-129 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: The microstructures of a poly(vinylcarbazole-g-isoprene) and blend of poly(vinylcarbazole) (PVCz) and polyisoprene (PIP) were studied by transmission electron microscopy (TEM). In the graft copolymer, the unique microphase separated structure was observed. In the blend, the blend ratio did not correspond to the area ratio on the TEM photograph. It is suggested that the results are caused by rigid and crystalline PVCz and low glass-transition temperature of PIP. © 1995 John Wiley & Sons, Inc.
    Additional Material: 3 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1995.070550114
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    Paper (German National Licenses)
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  • 5
    Electronic Resource
    Electronic Resource
    Microphase separation and crystallization of crystalline-amorphous type block copolymer. I. Effect of solvent (1993)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 48 (1993), S. 509-519 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: The formation process of the microphase separation and crystallization of a crystallineamorphous type diblock copolymer [poly(tetrahydrofuran-b-isoprene)] in solution were studied by transmission electron microscope and wide-angle X-ray diffraction measurements. The morphologies formed from three kinds of solvent systems are discussed in relation to the crystallization of poly(tetrahydrofuran) sequence. © 1993 John Wiley & Sons, Inc.
    Additional Material: 8 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1993.070480315
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  • 6
    Electronic Resource
    Electronic Resource
    Microphase separation and crystallization of crystalline-amorphous type block copolymer. VI. Crystalline part in crystalline domain (1994)
    New York, NY [u.a.] : Wiley-Blackwell
    Journal of Applied Polymer Science 51 (1994), S. 1709-1714 
    Details
    ISSN: 0021-8995
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: The crystalline and amorphous areas in poly(tetrahydrofuran) (PTHF) domains in a poly(tetrahydrofuran-b-isoprene) (crystalline-amorphous, PTHF = 52 wt %) film were distinguished by transmission electron microscopy and the relation between the crystallization and domain shape was clarified. The ratio of PTHF domain containing amorphous area was low in the case of the fewer interfaces of the small curvature formed by poly(isoprene) domain. The PTHF crystallization was closely related to the interface shape. © 1994 John Wiley & Sons, Inc.
    Additional Material: 8 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/app.1994.070511003
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    Paper (German National Licenses)
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