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  • Crystal structure  (2)
  • International Diagnostic Checklists (IDCL)  (2)
  • 1
    Digitale Medien
    Digitale Medien
    Reaktionen cyclischer Oxalylverbindungen, 34. Mitt.: Synthese von Dibenzoylacet-N-carboxyalkylamiden und semiempirische Rechnungen zur Keto-Enol Tautomerie (1992)
    Springer
    Monatshefte für Chemie 123 (1992), S. 265-275 
    Details
    ISSN: 1434-4475
    Schlagwort(e): 4-Benzoyl-5-phenylfuran-2,3-dione ; Dibenzoylacetic acid-N-carboxyamides ; Oxazin-2,4-dione ; Keto-enole tautomerism ; Semiempirical quantum chemical calculations ; Crystal structure
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Chemie und Pharmazie
    Notizen: Summary 4-Benzoyl-5-phenylfuran-2,3-dione (1) and the urethanes2 combine under loss of carbon monoxide yielding the open chain dibenzoylacetic acid derivatives3 and4. 3a, b only can be cyclized to the oxazinone5. The keto-enole tautomerism3 ⇌4 is further investigated with aid of semiempirical quantum chemical calculations, based upon the molecular geometry of3a, deduced from an X-ray study.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1007/BF00810475
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  • 2
    Digitale Medien
    Digitale Medien
    A five-coordinate copper complex with superoxide dismutase mimetic activity fromStreptomyces antibioticus (1988)
    Springer
    BioMetals 1 (1988), S. 112-116 
    Details
    ISSN: 1572-8773
    Schlagwort(e): Cu-desferrithiocin ; Crystal structure ; Superoxide dismutase activity ; Stability
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Biologie , Chemie und Pharmazie
    Notizen: Summary A Cu(II) complex of desferrithiocin fromStreptomyces antibioticus was prepared and characterized. The first shell atoms, including one nitrogen and four oxygens, were arranged around the copper in a square-planar pyramide. Due to the axially Jahn-Teller-distorted Cu-O distance at 224.7 pm, a distinct Cu2Zn2superoxide dismutase mimetic activity was measured. The Cu-complex survived 600 μM bovine serum albumin and the thermodynamic stability (pK=17.4) was not very different from that of Cu-EDTA. The electronic absorption properties, circular dichroism and electron paramagnetism were in accordance with those of the type-II copper species.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1007/BF01138069
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  • 3
    Digitale Medien
    Digitale Medien
    Routine psychiatric examinations guided by ICD-10 Diagnostic Checklists (International Diagnostic Checklists) (1993)
    Springer
    European archives of psychiatry and clinical neuroscience 242 (1993), S. 218-223 
    Details
    ISSN: 1433-8491
    Schlagwort(e): Classification ; ICD-10 ; International Diagnostic Checklists (IDCL)
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Medizin
    Notizen: Summary A systematic assessment of psychiatric diagnoses according to the new classification system ICD-10 can be guided and enhanced by the International Diagnostic Checklists (IDCL). This instrument was developed and evaluated primarily for use in routine clinical care. It consists of 30 separate lists in pocket form, each assigned to a specific disorder and allowing immediate and operationalized diagnostic decisions (without the need of computer assistance). Personality disorders are covered by a separate 12-page booklet (IDCL-P). Examples of the checklists are given together with possible areas of application. First studies have indicated good clinical practicability and satisfactory to excellent diagnostic reliability.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1007/BF02189966
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  • 4
    Digitale Medien
    Digitale Medien
    An empirical comparison of diagnoses and reliabilities in ICD-10 and DSM-III-R (1993)
    Springer
    European archives of psychiatry and clinical neuroscience 242 (1993), S. 209-217 
    Details
    ISSN: 1433-8491
    Schlagwort(e): Classification ; ICD-10 ; DSM-III-R ; Reliability ; Case Records ; International Diagnostic Checklists (IDCL)
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Medizin
    Notizen: Summary The psychiatric classification systems ICD-10 and DSM-III-R were compared by applying both sets of diagnostic criteria to the same sample of patients suffering from affective and psychotic disorders. Four independent raters assessed diagnoses according to both systems to 100 written case records which had been prepared in a traditional, standard format. The International Diagnostic Checklists (IDCL) were employed to rate relevant psychopathological signs and symptoms and to apply diagnostic decision rules. The results showed that ICD-10 yielded a generally higher reliability for all main disorders except for bipolar disorder. Overall reliability was κ=0.53 for diagnoses according to DSM-III-R and 0.59 for diagnoses according to ICD-10. Agreement was best for affective disorders, moderate for schizophrenia and inacceptable for schizoaffective disorder. Insufficient boundaries were found in both systems between schizoaffective disorder on one side and schizophrenia and bipolar disorder on the other side. The different duration criteria for schizophrenia of six months in DSM-III-R and one month in ICD-10 tend to have considerable consequences for frequency rates of schizophrenia in a typical clinical setting.
    Materialart: Digitale Medien
    URL: http://dx.doi.org/10.1007/BF02189965
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