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  • Dynamic mechanical analysis  (1)
  • ultrahigh molecular weight polyethylene fiber  (1)
  • 1
    ISSN: 1572-8935
    Keywords: Acrylic bone cement ; Ultra-high molecular weight polyethylene fiber ; Mechanical properties ; Dynamic mechanical analysis
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology , Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics , Physics
    Notes: Abstract The effects of the addition of ultra-high molecular weight polyethylene fiber (UHMWPE) on the mechanical properties of standard surgical Simplex-P radiopaque bone cement have been investigated. It was found that the tensile strength and tensile modulus were apparently not improved by the incorporation of UHMWPE in the acrylic bone cement. The results of bending strength and bending modulus indicated that a reinforcing effect is obtained at UHMWPE contents as low as 1 wt%, and then levelled off with increasing UHMWPE contents. When the UHMWPE contents as low as 2 wt%, the values of compressive strength and modulus seemed approximate the same; whereas the values of compressive strength and modulus decreased with increasing UHMWPE contents. From the results of dynamic mechanical analysis (DMA), the values of dynamic storage modulus of bone cement increased at UHMWPE fiber as low as 2 wt%, but beyond that UHMWPE content the value of the dynamic storage modulus decreased with increasing UHMWPE contents. The same results were also found for the dynamic loss modulus. When methyl methacrylate was grafted onto UHMWPE by plasma and UV irradiation treatment, it was found that by adding the treated UHMWPE fiber in acrylic bone cement had a significant reinforcing effect on the mechanical properties of bone cement.
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    Hoboken, NJ : Wiley-Blackwell
    Journal of Biomedical Materials Research 38 (1997), S. 361-369 
    ISSN: 0021-9304
    Keywords: acrylic bone cement ; ultrahigh molecular weight polyethylene fiber ; methyl methacrylate ; grafting ; mechanical properties ; Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Medicine , Technology
    Notes: Ultrahigh molecular weight polyethylene (UHMWPE) fibers were treated with argon plasma for 5 min, followed by uv irradiation in methyl methacrylate (MMA)-chloroform solution for 5 h to obtain MMA-g-UHMWPE grafted fiber. The grafting content was estimated by the titration of esterification method. The grafting amount of 5280 nmol/g was the largest for the MMA concentration at 18.75 vol%. To improve the mechanical properties of acrylic bone cement, pure UHMWPE fiber and MMA-g-UHMWPE fiber were added to the surgical Simplex®-P radiopaque bone cement. The mechanical properties including tensile strength, tensile modulus, compressive strength, bending strength, and bending stiffness were measured. Dynamic mechanical analysis was also performed. By comparing the effect of the pure UHMWPE fiber and MMA-g-UHMWPE grafted fiber on the mechanical properties of acrylic bone cement, it was found that the acrylic bone cement with MMA-g-UHMWPE grafted fiber had a more significant reinforcing effect than that with untreated UHMWPE fiber. This might be due to the improvement of the interfacial bonding between the grafted fibers and the acrylic bone cement matrix. © 1997 John Wiley & Sons, Inc. J Biomed Mater Res (Appl Biomater) 38: 361-369, 1997
    Additional Material: 8 Ill.
    Type of Medium: Electronic Resource
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