ISSN:
0268-2605
Keywords:
Ethylation
;
analysis
;
organotins
;
sodium tetraethylborate
;
tributyltin
;
tricyclohexyltin
;
triphenyltin
;
gas chromatography
;
mass spectroscopy
;
atomic absorption
;
Chemistry
;
Industrial Chemistry and Chemical Engineering
Source:
Wiley InterScience Backfile Collection 1832-2000
Topics:
Chemistry and Pharmacology
Notes:
A range of organotin compounds has been ethylated using the reagent sodium tetraethylborate in a simple one-step procedure. Analysis of the volatile, fully alkylated derivatives has been achieved by GC AA with confirmation of the identity of the resulting ethylated derivatives by GC MS. Conditions for the GC AA and GC MS analysis of the organometallic ethyl derivatives are given.
Additional Material:
8 Ill.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1002/aoc.590050306
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