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Funktionalisierte OctabisvaleneHerrn Professor Michael Hanack zum 60. Geburtstag gewidmet. (1991)

Trupp, BjöRn ; Handreck, Dirk-Rainer ; Böhm, Hans-Peter ; [et al.]

Weinheim : Wiley-Blackwell

Berichte der deutschen chemischen Gesellschaft 124 (1991), S. 1757-1775

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ISSN: 0009-2940

Keywords: Octabisvalene, 3-, 2,3-, and (Z)-3,7-(di)functionalized derivatives ; NMR Analysis, 13C,13C coupling constants ; Chemistry ; Inorganic Chemistry

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: Functionalized OctabisvalenesQuadricyclanone (13) is the starting material for a five-step synthesis of 3-cyanooctabisvalene (24, 19% total yield), cyclooctatetraene for a six-step synthesis of (Z)-3,7-dicyanooctabisvalene (58, 7% total yield). By decyanation of 24, the parent octabisvalene (1) is produced. NMR data, including 13C,13C coupling constants, are presented.

Additional Material: 1 Ill.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/cber.19911240814

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