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  • 1
    Electronic Resource
    Electronic Resource
    Darstellung und Kristallstruktur von [(Me3SiCH2)2InP(H)Ad]2Herrn Professor Peter Satori zum 60. Geburtstage gewidmet (1992)
    Weinheim : Wiley-Blackwell
    Zeitschrift für anorganische Chemie 611 (1992), S. 92-94 
    Details
    ISSN: 0044-2313
    Keywords: Indium-phosphorus four-membered ring ; phosphide ; phosphorus-indium bond ; phosphorus-hydrogen bond ; Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Description / Table of Contents: Preparation and Crystal Structure of [(Me3SiCH2)2InP(H)Ad]2Reaction of (Me3SiCH2)3 In with AdPH2 (Ad = adamantyl) in the presence of AgNO3 leads to [(Me3SiCH2)2InP(H)Ad]2 1 in 30% yield. The crystal structure of 1 is discussed.
    Notes: Die Reaktion von (Me3SiCH2)3 In mit AdPH2 (Ad = Adamantyl) führt in Gegenwart katalytischer Mengen AgNO3 unter Abspaltung von Tetramethylsilan in 30% Ausbeute zu [(Me3SiCH2)2InP(H)Ad]2 1. Die Kristallstruktur von 1 wird diskutiert.
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/zaac.19926110515
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    Paper (German National Licenses)
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  • 2
    Electronic Resource
    Electronic Resource
    Assignment of proton and carbon NMR signals of didemnin A in solution (1988)
    Chichester : Wiley-Blackwell
    Organic Magnetic Resonance 26 (1988), S. 501-506 
    Details
    ISSN: 0749-1581
    Keywords: Cyclic depsipeptide ; Inverse COLOC ; Inverse HMQC ; Semi-selective excitation ; NMR assignments in peptides ; Didemnin ; Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Several one- and two-dimensional techniques have been used to assign the 1H and 13C NMR spectra of the cyclic heptadepsipeptide didemnin A in DMSO. The composition and sequence of the amino acid residues was known beforehand and could be confirmed by heteronuclear proton-carbon long-range couplings using the COLOC experiment and a recently proposed new inverse technique using Gaussian-shaped pulses. The aliphatic methyl resonances of the isostatin, hydroxyisovalerylpropionyl, N-methylleucine and leucine residues were assigned by means of the TOCSY and NOESY techniques. Aliphatic carbon assignment was performed by inverse correlation via heteronuclear double quantum coherence.
    Additional Material: 5 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/mrc.1260260613
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    Paper (German National Licenses)
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