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  • 1
    Digitale Medien
    Digitale Medien
    Springer
    International journal of thermophysics 20 (1999), S. 721-731 
    ISSN: 1572-9567
    Schlagwort(e): effective emissivity ; specific heat capacity ; thermal radiation calorimetry
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Physik
    Notizen: Abstract A novel method for measurement of the specific heat capacity in the temperature range from 150 to 310 K is described. In order to achieve good temperature homogeneity in a disk-shaped specimen, a cylindrical heater was used in an apparatus based on thermal radiation calorimetry. A mixture of Bi2O3 and MgO powders was used for blackening the surfaces of the specimen, the heater, and the inside wall of the chamber. The specific heat capacities of Ni, fused quartz glass, and BaTiO3 ceramic were measured to test the performance of the calorimeter. Agreement to within 5% of the values published in the literature was obtained for these samples. Thermal hysteresis and anomalies associated with the first-order phase transition in BaTiO3 were detected in the present experiment.
    Materialart: Digitale Medien
    Bibliothek Standort Signatur Band/Heft/Jahr Verfügbarkeit
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  • 2
    Digitale Medien
    Digitale Medien
    Springer
    International journal of thermophysics 21 (2000), S. 927-940 
    ISSN: 1572-9567
    Schlagwort(e): calorimetry ; emittance ; fused silica ; hemispherical total emissivity ; refractive index ; spectral emissivity ; thermal conductivity ; virtual mode ; Vycor glass
    Quelle: Springer Online Journal Archives 1860-2000
    Thema: Physik
    Notizen: Abstract An attempt to derive the hemispherical total emissivity from the normal emission spectrum is proposed for Vycor and fused silica glasses. The normal emission spectrum from a clear surface has been measured at steady state in the temperature range from 400 to 750 K. The sample is heated on one metal-backed face by thermal radiation from a heater. Temperatures inside the sample were monitored by thermocouples at two points near the surfaces. Evaluation of the hemispherical total emissivity from the normal emission spectrum is determined by means of Kramers–Krönig analysis and virtual mode equations. Assuming a linear temperature distribution within the sample, the thermal conductivities of silicate glasses were obtained at elevated temperatures. The results are comparable with those obtained by previous investigators. The effect of radiation heat transfer in a sample is also discussed.
    Materialart: Digitale Medien
    Bibliothek Standort Signatur Band/Heft/Jahr Verfügbarkeit
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