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  • 1
    Electronic Resource
    Electronic Resource
    Springer
    Catalysis letters 21 (1993), S. 309-320 
    ISSN: 1572-879X
    Keywords: Sol-gel catalysts ; platinum-tin catalysts ; platinum dispersion ; X-ray diffraction ; energy dispersive X-ray analysis ; EDX analysis
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Abstract Highly dispersed platinum was found in Pt-Sn/Al2O3 catalysts prepared by the sol-gel method, i.e., cogelation of aluminum tri-sec-butoxide and tetrabutyltin and subsequent impregnation with hexachloroplatinic acid. X-ray diffraction studies showed that the cell parameter of pure platinum is not modified in bimetallic Pt-Sn samples. Moreover, energy dispersive X-ray analysis studies (EDX) showed that platinum, but not tin, was detected in the catalysts where tin was incorporated by the sol-gel coprecipitation of tin and aluminum. Incorporation of tin into the alumina network is suggested.
    Type of Medium: Electronic Resource
    Library Location Call Number Volume/Issue/Year Availability
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  • 2
    Electronic Resource
    Electronic Resource
    Springer
    Journal of sol gel science and technology 8 (1997), S. 437-442 
    ISSN: 1573-4846
    Keywords: sol-gel hydrotalcites ; X-ray diffraction ; aluminum precursors ; hydrotalcites Mg/Al ratio ; mixed metal hydroxides
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Abstract Sol-Gel Hydrotalcites were synthesized using magnesium ethoxide and variable aluminum sources: aluminum acetilacetonate, aluminum chloride, aluminum nitrate and aluminum sulfate; in all cases, the gelation was done at pH 10. X-ray diffraction studies show that the crystallinity depends on the aluminum precursor used. The crystallinity was found in the order aluminum acetylcetonate 〉 aluminum chloride 〉 aluminum nitrate 〉 aluminum sulfate. The precursor determines the sintering behavior as well.
    Type of Medium: Electronic Resource
    Library Location Call Number Volume/Issue/Year Availability
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  • 3
    Electronic Resource
    Electronic Resource
    Springer
    Journal of sol gel science and technology 8 (1997), S. 437-442 
    ISSN: 1573-4846
    Keywords: sol-gel hydrotalcites ; X-ray diffraction ; aluminum precursors ; hydrotalcites Mg/Al ratio ; mixed metal hydroxides
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Abstract Sol-Gel Hydrotalcites were synthesized using magnesium ethoxide and variable aluminum sources: aluminum acetilacetonate, aluminum chloride, aluminum nitrate and aluminum sulfate; in all cases, the gelation was done at pH 10. X-ray diffraction studies show that the crystallinity depends on the aluminum precursor used. The crystallinity was found in the order aluminum acetylcetonate〉aluminum chloride〉aluminum nitrate〉aluminum sulfate. The precursor determines the sintering behavior as well.
    Type of Medium: Electronic Resource
    Library Location Call Number Volume/Issue/Year Availability
    BibTip Others were also interested in ...
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