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Chromatographic resolution of chiral intermediates in β-adrenergic blocker synthesis on chiral stationary phases (1993)

Ader, Ulrich ; Muschalek, Volker ; Schneider, Manfred P.

New York, NY [u.a.] : Wiley-Blackwell

Chirality 5 (1993), S. 554-559

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Details

ISSN: 0899-0042

Schlagwort(e): HPLC ; chiral stationary phases ; resolution of enantiomers ; β-adrenergic blockers ; alcohols ; acetates ; Chiralcel OB ; Chiralcel OD ; Chiralpak OT(+) ; Chemistry ; Organic Chemistry

Quelle: Wiley InterScience Backfile Collection 1832-2000

Thema: Chemie und Pharmazie

Notizen: The enantiomeric purities of optically active intermediates for β-adrenergic blocking agents prepared via enzyme-assisted processes can be determined rapidly and with high accuracy using HPLC on commercially available columns with chiral supports [Chiralcel OD, OB; Chiralpak OT(+)]. The dependence of the resolution parameters on the substitution pattern of both hydroxy compounds and their esters is reported. © 1993 Wiley-Liss, Inc.

Zusätzliches Material: 2 Ill.

Materialart: Digitale Medien

URL: http://dx.doi.org/10.1002/chir.530050712

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