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Substituted aza and aza-thia macrocycles: An example of a calamitic macrocyclic metallomesogen (1994)

Neve, Francesco ; Ghedini, Mauro

Springer

Journal of inclusion phenomena and macrocyclic chemistry 15 (1994), S. 259-272

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ISSN: 1573-1111

Keywords: Metallomesogens ; liquid crystals ; aza-thia macrocycles ; azacrowns

Source: Springer Online Journal Archives 1860-2000

Topics: Chemistry and Pharmacology

Notes: Abstract The new bis-4-(hexyloxy)benzamide and bis-4-(dodecyloxy)benzamide derivatives of macrocyclic ligands [18]aneN2O4 (L1 and L2) and [18]aneN2S4 (L3 and L4) have been prepared and characterized by1H and13C NMR spectroscopy, differential scanning calorimetry and optical microscopy. The nonmesogenic ligands L3 and L4 react with [Pd(CH3CN)4][BF4]2 to give the cationic complexes [Pd(L3)][BF4]2 and [Pd(L4)][BF4]2. [Pd(L4)][BF4]2 shows mesomorphic behaviour affording a smectic mesophase.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1007/BF00709071

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