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  • spray pyrolysis  (2)
  • bioactivity  (1)
  • 1
    ISSN: 1573-4846
    Keywords: spray pyrolysis ; apatite ; composite particle ; biomimetic deposition
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Abstract Apatite derived by sol-gel routes through an amorphous state or derived biomimetically is likely to provide chemically and biologically active surfaces. Thus apatite or apatite-composite particles were prepared by spray-pyrolysis of several solutions as they were applicable to medical treatment. Calcium lactate and ammonium dihydrogen phosphate aqueous solutions stabilized with ethylenediaminetetraacetic acid were sprayed ultrasonically and pyrolysed at 600°C to yield amorphous particles of apatite while apatite-ferric oxide composite powders were prepared from the solutions of calcium lactate and ferric nitrate. Solutions of calcium nitrate and titanium ethoxide in 0.5 N HNO3 were also spray-pyrolysed at 600°C to prepare calcium titanate and titanium oxide particles trapped on a Ti substrate. Apatite could biomimetically be developed on the calcium titanate particles when they were soaked in an acellular simulated body fluid.
    Type of Medium: Electronic Resource
    Library Location Call Number Volume/Issue/Year Availability
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  • 2
    ISSN: 1573-4846
    Keywords: spray pyrolysis ; apatite ; composite particle ; biomimetic deposition
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Abstract Apatite derived by sol-gel routes through an amorphous state or derived biomimetically is likely to provide chemically and biologically active surfaces. Thus apatite or apatite-composite particles were prepared by spray-pyrolysis of several solutions as they were applicable to medical treatment. Calcium lactate and ammonium dihydrogen phosphate aqueous solutions stabilized with ethylenediaminetetraacetic acid were sprayed ultrasonically and pyrolysed at 600°C to yield amorphous particles of apatite while apatite-ferric oxide composite powders were prepared from the solutions of calcium lactate and ferric nitrate. Solutions of calcium nitrate and titanium ethoxide in 0.5 N HNO3 were also spray-pyrolysed at 600°C to prepare calcium titanate and titanium oxide particles trapped on a Ti substrate. Apatite could biomimetically be developed on the calcium titanate particles when they were soaked in an acellular simulated body fluid.
    Type of Medium: Electronic Resource
    Library Location Call Number Volume/Issue/Year Availability
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  • 3
    Electronic Resource
    Electronic Resource
    Springer
    Journal of sol gel science and technology 13 (1998), S. 237-240 
    ISSN: 1573-4846
    Keywords: coating ; bioactivity ; apatite ; Ca incorporation ; silianol groups
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Abstract An ethanol (EtOH) solution of polymerized vinyltrimethoxysilane (VTMS), about 20-mers, was mixed with an aqueous solution of calcium acetate (Ca(OAc)2) and refluxed in N2 for 1 h to give sols of a typical composition VTMS : H2O : EtOH : Ca(OAc)2 = 1 : 9 : 8 : 0.05 (mol). Homogeneous films could be produced, by dip-coating, on Nylon6® and soda-lime glass, but not on polypropylene or polytetrafluoroethylene. The gel films did not deposit apatite within 14 days of soaking in a simulated body fluid whereas films abraded with emery paper as well as bulk gels deposited apatite on the surfaces within 7 days, indicating the present gel was suitable for bioactive coatings on Nylon6®
    Type of Medium: Electronic Resource
    Library Location Call Number Volume/Issue/Year Availability
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