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  • 1
    Electronic Resource
    Electronic Resource
    Molecular structure of AlH3[N(CH2CH2)3CH]2 (1998)
    Springer
    Journal of chemical crystallography 28 (1998), S. 649-651 
    Details
    ISSN: 1572-8854
    Keywords: Crystal structure ; aluminum ; hydride ; complex ; quinuclidine
    Source: Springer Online Journal Archives 1860-2000
    Topics: Geosciences , Physics
    Notes: Abstract Reaction of AlH3[N(CH2CH2)3CH] with hexamethyltrisiloxane, (OSiMe2)3, gives rise to the bis-quinuclidine complex AlH3[N(CH2CH2)3CH]2, which has been characterized by 1H and 13C NMR spectroscopy and X-ray crystallography. The molecular structure of AlH3[N(CH2CH2)3CH]2 consists of a trigonal bipyramidal aluminum with axial coordination of the quinuclidine ligands. Crystal data: orthorhombic, space group Pbcn, a = 10.6895(9), b = 12.266(1), c = 12.3794(9) Å, V = 1623.2(2) Å3, and Z = 4.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1023/A:1022473312315
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    Paper (German National Licenses)
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  • 2
    Electronic Resource
    Electronic Resource
    Molecular structure of (tBu)3Al[O=C(OPh)2] (1999)
    Springer
    Journal of chemical crystallography 29 (1999), S. 993-996 
    Details
    ISSN: 1572-8854
    Keywords: aluminum ; carbonate ; complex
    Source: Springer Online Journal Archives 1860-2000
    Topics: Geosciences , Physics
    Notes: Abstract The molecular structure of (tBu)3Al[O=C(OPh)2] has been determined. The increase in the C=O bond distance [1.258(4) Å] when compared to free O=C(OPh)2 [1.191(3) Å], is presented in respect to the activating ability of aluminum Lewis acids. Crystal data: monoclinic, P21/n, a = 10.653(2), b = 18.486(4), c = 14.551(3) Å, β = 108.07(3)°, and V = 2724.3(9) Å3 for Z = 4.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1023/A:1009546631156
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    Paper (German National Licenses)
    Fulltext
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