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Catalytic polarographic detection of disulfides following liquid chromatography (1992)

Nagashima, Kunio ; Kamaya, Minori ; Ishii, Eizen

Weinheim : Wiley-Blackwell

Electroanalysis 4 (1992), S. 245-247

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ISSN: 1040-0397

Keywords: Disulfides ; flow detector ; polarography ; Chemistry ; Polymer and Materials Science

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: Four kinds of disulfides in organic compounds were sensitively detected in NH4OH-NH4Cl (0.2 M)-Co2+ (5 × 10-4 M) solution by differential-pulse polarography. This detection mechanism was based on the Brdicka reaction. A new flow-through cell (on-detector reactor) was used to combine the polarographic detection with high-performance liquid chromatography. The detection limit for dithioglycolic acid was 1 × 10-4 M using 10 μl samples.

Additional Material: 3 Ill.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/elan.1140040216

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