ISSN:
0935-6304
Keywords:
Liquid chromatography
;
Gas chromatography
;
LC/GC
;
On-line coupling
;
Metal complexes
;
Chemistry
;
Analytical Chemistry and Spectroscopy
Source:
Wiley InterScience Backfile Collection 1832-2000
Topics:
Chemistry and Pharmacology
Notes:
The on-line coupled LC-GC technique was applied to the analysis of several metal chelates of N,N-diethyldithiocarbamic acid. A 10-port valve interface was used to couple the LC and GC instruments. Conditions during sample transfer into the GC gave fully concurrent solvent evaporation. The chelates investigated were separated with a short apolar fused silica column. LC preseparation was made with cyano or amino phases using a hexane/dichloromethane mixture as eluent. On-line LC-GC combination seems to be very suitable for the separation of the metal chelates studied.
Additional Material:
5 Ill.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1002/jhrc.1240130306
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