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  • 1
    Electronic Resource
    Electronic Resource
    Herstellung, optische Reinheit und Konfiguration der Flecainid-Enantiomeren (1985)
    Weinheim : Wiley-Blackwell
    Berichte der deutschen chemischen Gesellschaft 118 (1985), S. 4616-4619 
    Details
    ISSN: 0009-2940
    Keywords: Chemistry ; Inorganic Chemistry
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: Preparation, Optical Purity and Configuration of the Enantiomers of FlecainideThe chiral antiarrhythmic drug flecainide (rac-1) was resolved by fractional crystallization of the diastereomeric salts with optically active mandelic acid. Derivatization with (+)-1-phenylethyl isocyanate and analytical separation of the diastereomers 3 by HPLC on silica gel confirmed the optical purity of the enantiomers. CD-Spectra of the N-chloro derivatives established the absolute configuration: (-)-1 is R-, (+)-1 S-configurated.
    Additional Material: 1 Ill.
    Type of Medium: Electronic Resource
    URL: http://dx.doi.org/10.1002/cber.19851181132
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