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  • 1
    Digitale Medien
    Digitale Medien
    Oxford, UK : Blackwell Science Inc
    Journal of the American Ceramic Society 88 (2005), S. 0 
    ISSN: 1551-2916
    Quelle: Blackwell Publishing Journal Backfiles 1879-2005
    Thema: Maschinenbau , Physik
    Notizen: The effect of the amount of the sintering additives, i.e., yttria and alumina, on the microstructure and the high-temperature flexural strengths of silicon nitride with and without the aligned whisker seeds was examined. As the amount of the sintering additives was increased, both width and length of the grains were increased. The high-temperature strengths of silicon nitride with and without the aligned seeds were increased and decreased, respectively, according to the increase of the amount of the sintering additives. When both 4.8 wt% yttria and 2.2 wt% alumina were added to silicon nitride with the aligned whisker seeds, the experimental results indicated that it had three times the flexural strength as silicon nitride without the seeds at 1673 K. During the high-temperature flexure testing, observations did not indicate yielding present in the samples with the aligned whisker seeds, while it was present in samples without the whisker seeds. The reinforcing grains growing from the whisker seeds aligned perpendicular to the crack propagation direction acted as effective obstacles to the crack propagation and improved the fracture toughness.
    Materialart: Digitale Medien
    Bibliothek Standort Signatur Band/Heft/Jahr Verfügbarkeit
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  • 2
    Digitale Medien
    Digitale Medien
    Westerville, Ohio : American Ceramics Society
    Journal of the American Ceramic Society 86 (2003), S. 0 
    ISSN: 1551-2916
    Quelle: Blackwell Publishing Journal Backfiles 1879-2005
    Thema: Maschinenbau , Physik
    Notizen: Silicon nitride ceramics seeded with 3 wt%β-Si3N4 whiskers of two different sizes were prepared by a modified tape casting and gas pressure sintering. The fine whiskers had a higher aspect ratio than the coarse whiskers. Quantitative texture analysis including calculation of the orientation distribution function (ODF) was used for obtaining the degrees of preferred orientation of sintered samples. The maximum multiples of random distribution (mrd) values of samples seeded with the fine and coarse whiskers were large, greater than 15 and 9, respectively. Meanwhile, the mrd value of a sample seeded with fine whiskers was only 9 when it was prepared by conventional tape casting. The microstructures and the XRD data revealed that the well-aligned whiskers grew significantly after sintering and dominated the texture. Differences among the degrees of preferred orientation of the samples were explained using Jeffrey's model on rotation of elliptical particles carried by a viscous fluid.
    Materialart: Digitale Medien
    Bibliothek Standort Signatur Band/Heft/Jahr Verfügbarkeit
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