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  • 1
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Solid state phenomena Vol. 141-143 (July 2008), p. 475-480 
    ISSN: 1662-9779
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Physics
    Notes: The aim of this work is to study by X-Ray microtomography carried out at ESRFGrenoble the microstructure of an Al-4wt%Cu alloy which was previously cold rolled to obtainglobules of the solid phase upon heating in the semi-solid range. Since this process producedentrapped liquid in the globules, 3D quantification of this liquid was performed. Moreover, theinfluence of the addition to the alloy of a small amount of Ba, which has been shown to decrease thecontiguity between the solid globules as a consequence of the decrease of the solid-liquid interfacialenergy σsl, was investigated. It is in particular shown that the amount of entrapped liquid is muchlarger in the Ba-containing alloy in agreement with the reduction of σsl, whereas the size of theliquid pockets is similar. In addition characterization of the interglobular liquid shows that theinterface area between this liquid and the solid per unit volume is larger for the alloys containing Bain agreement with previous observations carried out on 2D sections. The influence of strain duringcold rolling is also reported but it is shown to have a quite limited influence on the previousparameters
    Type of Medium: Electronic Resource
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  • 2
    ISSN: 1662-9752
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Reliability of functionally graded metal matrix composites (FGMMCs) for automotive components is still dependent on the detailed knowledge of the mechanisms of the microstructural build-up, for instance on the mechanisms leading to the distribution and relative positions of the reinforcing particles. In order to assess the influence of the SiC particle size on the 3-D inter-particle connectivity in functionally graded Al/SiCp composites produced by centrifugal casting, X-raymicrotomography experiments were performed at the ID19 beamline in ESRF (European Synchrotron Radiation Facility). The FGMMCs consisted of an Al-10Si-2Mg alloy matrix, reinforced by an average SiC particle volume fraction of 0.10; two different average sizes were used: 37 µm and 12 µm. The holographic modification of the X-ray CMT (Computer Micro- Tomography) method allowed to obtain neatly contrasted images, as opposed to classical CMT.Good agreement was found between the particle size evaluated by CMT and by laser interferometry. Particle clustering has been evaluated in number and volume, showing that a lowermean particle size is related to more clustering. Such an adverse effect relies on the importance of particle/liquid alloy surface tension. Also, the mean particle size has been evaluated as a function of particle number within a cluster: as expected, the larger a cluster, the larger the particles inside it
    Type of Medium: Electronic Resource
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