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  • 1
    ISSN: 1662-9752
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Many researchers became interested in the discovery of Bi2Sr2CaCu2O8+δ oxides withcritical temperature of around 80 K. It is known that the critical temperature is related to the CuO2planes of the material. For this reason, the study of the interstitial oxygen in these oxides is of greatrelevance. The samples were prepared by means of conventional solid state reactions, through thestoichiometric mixture of precursory powders. After the sinterization, the samples were submittedto measurements of density, electrical resistivity, x-ray diffraction, scanning electron microscopyand energy dispersion spectroscopy, with the objective of performing their characterization. Themeasurements of mechanical spectroscopy were performed by a torsion pendulum. The resultsshow three relaxation processes in the temperature range of 200 and 700 K, with activation energyof approximately 0.9 eV, which has been attributed to the dynamics of the interstitial oxygenpresent in the material
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Materials science forum Vol. 591-593 (Aug. 2008), p. 644-648 
    ISSN: 1662-9752
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: A new class of hybrid ruteno-cuprates – such as Ru-1212 and Ru-1222 – was discoveredin 1995 by Bauerfeind and collaborators. These materials present superconducting and magneticstates at low temperatures, an atypical duality in other superconductors. The superconductivity ismore easily observed in Ru-1222, while Ru-1212 is a more problematic case, due to the strongeffects of the preparation details in its superconducting properties, becoming the materialsuperconductor or not. Ru-1212 presents a critical temperature that can vary between 0 and 46 K,depending on the preparation conditions, and a temperature of magnetic transition of around 132 K.The samples were prepared through solid state reactions, by using a mixture of high purity powders,followed by calcination and sinterization in the nitrogen and oxygen atmospheres. This paper showsthe preparation process of Ru-1212 samples, followed by their structural and magneticcharacterization
    Type of Medium: Electronic Resource
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