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Structure refinement and Raman spectrum of silver azide (1999)

Guo, Guo-Cong ; Wang, Quan-Ming ; Mak, Thomas C.W.

Springer

Journal of chemical crystallography 29 (1999), S. 561-564

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ISSN: 1572-8854

Keywords: crystal structure ; Raman spectrum ; silver azide ; azide

Source: Springer Online Journal Archives 1860-2000

Topics: Geosciences , Physics

Notes: Abstract Silver nitrate reacts with sodium azide to give white powdery silver azide, which can be crystallized in aqueous ammonia. The compound belongs to orthorhombic space group Ibam with a = 5.600(1), b = 5.980(6), c = 5.998(1) Å, and Z = 4. The layer-type structure is constructed from edge-sharing regular rectangles, each composed of silver atoms at its vertices with an enclosed azide anion in a tilted orientation. The linear and asymmetrical structure of the azide anion in crystalline silver azide has been confirmed by its Raman spectrum.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1023/A:1009544702195

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