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High temperature (GC)2 and (GC)2/CI-MS of nucleosides: Analysis of purinyl nucleoside isomer composition (1980)

Fischer, P. ; Lösch, G. R. ; Müller, D.

Weinheim : Wiley-Blackwell

Journal of High Resolution Chromatography 3 (1980), S. 161-165

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ISSN: 0935-6304

Keywords: GC, GC/MS ; Capillary, HMDS-deactivated ; On-column injection ; Nucleoside linkage isomers ; Separation, structural assignment feasibilities ; Chemistry ; Analytical Chemistry and Spectroscopy

Source: Wiley InterScience Backfile Collection 1832-2000

Topics: Chemistry and Pharmacology

Notes: The analysis of low-volatile polar nucleosides by (GC)2/FID and (GC)2/CI-MS, employing HMDS-deactivated glass capillary columns and on-column injection, is described. The four linkage isomers of a specific nucleoside, formed in the synthetic procedure, are in each case sufficiently well separated in the chromatogram; GC/CI-MS allows for a differentiation of N-7 and N-9 linkage isomers.

Additional Material: 4 Ill.

Type of Medium: Electronic Resource

URL: http://dx.doi.org/10.1002/jhrc.1240030402

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