ISSN:
0021-8383
Keywords:
Chemistry
;
Organic Chemistry
Source:
Wiley InterScience Backfile Collection 1832-2000
Topics:
Chemistry and Pharmacology
Notes:
A new method for the synthesis of homoschizokinen 1 and schizokinen 2 is described. 2-tert-Butyl-1,3-di-N-hydroxysuccinimidyl citrate has been applied as the key substrate. The method excludes the possibility of imide formation. The imide of compound 1 has been obtained analogously from the active ester of the 1,3-dioxolan-4-one derivative 5. It has been stated that 13C-n.m.r. signals of the C-3 carbon atoms enable the detection of traces of homoschizokinen 17.
Additional Material:
2 Tab.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1002/prac.19873290310
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