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  • 1
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 65 (1989), S. 3136-3141 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: The effects of uniaxial compression, high-temperature (920 °C) heat treatment, and heat treatment plus magnetic field on grain alignment in bulk ceramic pellets of HoBa2Cu3O7−δ and YBa2Cu3O7−δ were studied and separated. Uniaxially cold pressing prereacted powder into pellets at room temperature is found to yield significant grain alignment on the flat end surfaces of the pellets perpendicular to the pressing axis, where the c axes of the grains are parallel to this axis, in agreement with previous reports. A simple method to quantitatively determine the degree of surface grain alignment from the powder x-ray diffraction data from these surfaces is used. These data were augmented by x-ray rocking curve measurements. The degree of alignment of the cold pressed samples was found to increase with increasing pressure up to our pressure limit of 310 MPa. However, bulk magnetization anisotropy measurements on these pellets indicate that the degree of bulk alignment is only about 1/3 to 1/2 that inferred from the above surface measurements, which in turn suggests that the degree of alignment decreases with distance from the flat end surfaces. We find that a pronounced additional surface grain alignment is produced by heat treating the cold-pressed samples at high temperature (920 °C). We also observed a significant influence during the high-temperature annealing of a small (0.7 T) applied magnetic field on the alignment of the surface grains. A model to explain these observations is presented and discussed.
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    [S.l.] : American Institute of Physics (AIP)
    Journal of Applied Physics 74 (1993), S. 2076-2089 
    ISSN: 1089-7550
    Source: AIP Digital Archive
    Topics: Physics
    Notes: The frequency-dependent impedance of right-cylindrical air-core eddy-current probes over thick metal plates whose conductivity and permeability vary as a function of depth in the near-surface region have been studied both experimentally and theoretically. Measurements of probe impedance were made from 1 kHz to 1 MHz using an impedance analyzer. Precision-wound air-core coils were used for testing the theory, and commercial eddy-current probes were used to connect with industrial practice. The samples were of two types. First, to model a continuous profile, otherwise uniform plates of metal covered with many thin, discrete layers of other metals were considered. Second, as a practical example, case-hardened titanium plates, whose near-surface conductivity varies smoothly and continuously as a function of depth, were considered. Two theoretical results are presented for continuously varying profiles. First, an exact closed-form solution (within the quasistatic approximation) is reported for the impedance of a right-cylindrical air-core probe above a nonmagnetic metal whose near-surface conductivity difference varies as a hyperbolic tangent as a function of depth. Second, a new numerical technique is reported for determining the impedance of an air-core probe above a layered material whose conductivity and permeability vary arbitrarily. It is shown that the numerical technique converges and that for a hyperbolic tangent profile it agrees with the closed-form analytic solution and experiment. In general, it was found that continuous profiles can be experimentally (and theoretically) simulated by stacking many thin layers with differing conductivities, and that the probe's impedance change is larger if the conductivity change is localized at the surface, and is smaller for more diffuse profiles.
    Type of Medium: Electronic Resource
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