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  • 1
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Materials science forum Vol. 591-593 (Aug. 2008), p. 114-119 
    ISSN: 1662-9752
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Roller-ball milling (RBM) or planetary ball milling (PBM) have been used together withthe hydrogen decrepitation (HD) process to produce sintered permanent magnets based on a mixtureof Pr16Fe76B8 and Pr14.00Fe63.90Co16.00B6.00Nb0.10 magnetic alloys. Five distinct compositions havebeen studied comparing low- and high-energy milling. Magnets with a particular composition andprepared using these two routes exhibited similar magnetic properties. Modifications have beencarried out in the procedure of the HD stage for PBM in order to guarantee a high degree ofcrystallographic alignment. Pr15.00Fe69.95Co8.00B7.00Nb0.05 magnets showed the best maximum energyproduct for both processing routes (~ 247 kJm-3). A significant reduction in the milling time (93%)has been achieved with high-energy processing, the greatest advantage over the low-energy route
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Materials science forum Vol. 591-593 (Aug. 2008), p. 885-890 
    ISSN: 1662-9752
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Sintered magnets have been produced with powder obtained using the hydrogenation,disproportionation, desorption and recombination process (HDDR). The new processing procedurefor the production of the sintered magnets has been adopted in an attempt to reduce the millingtime. Commercial cast ingot alloys based on the compositions Pr14Fe75.9Co4B6Nb0.1 andPr20.5FebalB5Cu2.0 have been employed in this investigation. The HDDR powder was used toproduce sintered magnets using a mixture of these alloys, in very distinct proportions. Only a smallamount (20 wt. %) of the copper-containing alloy has been added as a sintering aid. Standardhydrogen decrepitation (HD) magnets have also been included in this work for a comparison. Theeffect of a reduced milling time on the magnetic properties of the HDDR sintered magnets has beeninvestigated. Sintering temperature and time of were kept constant for all magnets (1050ºC for 60minutes). The microstructures of the permanent magnets have been investigated by scanningelectron microscopy and energy dispersive X-ray analysis
    Type of Medium: Electronic Resource
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