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  • 1
    Electronic Resource
    Electronic Resource
    Copenhagen : International Union of Crystallography (IUCr)
    Applied crystallography online 5 (1972), S. 40-46 
    ISSN: 1600-5767
    Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001
    Topics: Geosciences , Physics
    Notes: In order to test the collimation correction methods routinely applied to small-angle X-ray scattering data, scattering curves for several samples have been obtained both with a Kratky camera and with a Beeman four-slit collimation system. Since the two collimation systems used quite different slit arrangements, there were appreciable differences in the measured curves obtained with the two systems for a given sample. However, after the appropriate collimation corrections had been applied, the corrected curves were nearly identical. This agreement, which is not surprising because of the thorough tests previously applied to collimation correction procedures, indicates that in the correction of experimental curves, no unforeseen problems appear that are not present in the earlier, more idealized tests, which employed test functions to simulate experimental curves. A comparison has been made of a few other properties of the two collimation systems, including the intensity obtainable for a given resolution.
    Type of Medium: Electronic Resource
    Library Location Call Number Volume/Issue/Year Availability
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  • 2
    Electronic Resource
    Electronic Resource
    Copenhagen : International Union of Crystallography (IUCr)
    Applied crystallography online 4 (1971), S. 50-55 
    ISSN: 1600-5767
    Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001
    Topics: Geosciences , Physics
    Notes: Two different small-angle X-ray scattering methods have been used to determine the electron density of the particles in a colloidal silica suspension. In the first method, the electron density of the particles was calculated from the measured change of the zero-angle scattered intensity caused by the addition of known quantities of sucrose to increase the solvent electron density. In the second method, the scattering from the suspension was compared with the scattering from a nearly ideal gas. Within an experimental uncertainty of about 5%, the electron density of the silica particles was found by both methods to have a value corresponding to pure SiO2 particles with the mass density 2.28 g.cm−3 which is listed in the manufacturer's literature describing the suspensions. This determination of the electron density will enable these suspensions to be used as standard samples in determinations of the ratio of the scattered intensity to the incident intensity.
    Type of Medium: Electronic Resource
    Library Location Call Number Volume/Issue/Year Availability
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