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  • 1
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Materials science forum Vol. 500-501 (Nov. 2005), p. 729-736 
    ISSN: 1662-9752
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: The effects of matrix microstructure and features of non-metallic inclusion (morphology, type, volume fraction and size) on cleavage initiation in medium-carbon Ti-V-N and V-N microalloyed resulphurized forging steels have been determined by examining fracture surfaces produced in room temperature Charpy impact tests. The steels were generally Al-deoxidised but one V-N steel was Si-deoxidised. It has been found that, in the Ti-treated steel, having a ferrite-pearlitemicrostructure, brittle fracture initiation occurred at cracked coarse (Ti,V)(C,N) single phase or [(Ti,V)(C,N)/Al2O3/MnS] multi-phase inclusions. In the Ti-free steels, cleavage initiation was dependent on matrix microstructure and non-metallic inclusions. In the low strength Ti-free steels, with a ferrite-pearlite microstructure, the absence of a continuous grain boundary ferrite layer led to initiation from interfacing pearlite colonies. For the bainitic microstructure, cleavage initiated close to the notch, but the microstructural feature responsible could not be identified. For the ferritepearlite microstructure in the Si-deoxidised V-N steel, cleavage initiated at cracked Mn-Al-(Ca) silicate inclusions. The higher matrix strength and more continuous nature of grain boundary allotriomorphic ferrite in the V-N steel deoxidised with Al was associated with cleavage initiation from V-rich (V,Ti)(C,N)-containing inclusions. These were generally of smaller size than those in the Ti-treated steels
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Materials science forum Vol. 500-501 (Nov. 2005), p. 613-622 
    ISSN: 1662-9752
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Bimodal grain size distributions were found in continuously cast slab and thermomechanical controlled rolled (TMCR) samples of Nb-microalloyed steel. Scanning electron microscopy (SEM) revealed inhomogeneous distributions of Al- and Nb-containing precipitates, which were found to pin prior austenite grain boundaries during reheating. An effort has been made to establish parameters to quantify the extent of bimodality of reheated and rolled microstructures. Quantification of bimodality using peak grain size range, (PGSR) and peak height ratio, (PHR), is found to match closely with the visual observation of bimodality. Thermo-Calc software was used to predict the sequence of precipitation for different compositions and that could explain the formation of bimodality during reheating
    Type of Medium: Electronic Resource
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  • 3
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Materials science forum Vol. 519-521 (July 2006), p. 641-646 
    ISSN: 1662-9752
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: AA5182 (Al-4.5 wt% Mg) can become susceptible to intergranular corrosion (IGC) withtime at moderately elevated service temperatures owing to precipitation of Mg-rich β-phase at grainboundaries, which can lead to stress corrosion cracking (SCC). The IGC and SCC susceptibility ofAA5182 was found to depend strongly on sensitisation heat treatments. AFM and TEM studiesdemonstrated that the degree of precipitation and thus susceptibility to attack for a boundary can berelated to its crystallographic misorientation. Low angle boundaries (〈20°) are most resistant toattack as they do not show β-phase precipitation. However, higher angle boundaries show highlyvariable precipitation and corrosion susceptibility: critical factors are the grain boundary plane andprecipitate/matrix crystallographic relationship
    Type of Medium: Electronic Resource
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  • 4
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Materials science forum Vol. 530-531 (Nov. 2006), p. 473-477 
    ISSN: 1662-9752
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Notes: Melt spun Ni-Cr-P alloy ribbons were used as filler metal to join Al2O3substrates together using a vacuum brazing process. The influence of the brazing load,brazing temperature and holding time on the shear resistance of brazed joints wasevaluated. The experimental results showed that the holding time was the mostimportant parameter. At a brazing temperature of 1060°C, the shear resistance valueincreased from 6.17 to 93.7 MPa with increasing brazing time from 20 to 100 min,respectively
    Type of Medium: Electronic Resource
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