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  • 1
    Electronic Resource
    Electronic Resource
    [s.l.] : Nature Publishing Group
    Nature 268 (1977), S. 711-713 
    ISSN: 1476-4687
    Source: Nature Archives 1869 - 2009
    Topics: Biology , Chemistry and Pharmacology , Medicine , Natural Sciences in General , Physics
    Notes: [Auszug] Fig. 1 Gas chromatograms obtained from a, 1-ml aliquot taken with heated syringe from a 180-ml glass bottle sealed with nylon film, containing 5ul paraffin and heated to 110 C; 6, induction heating for 10 s in the Curie point apparatus of an adsorption wire after 1.5h immersion in an identical ...
    Type of Medium: Electronic Resource
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  • 2
    ISSN: 1612-1112
    Keywords: Arson ; Curie point pyrolysis ; Air pollution ; Vapour sampling ; Capillary PC
    Source: Springer Online Journal Archives 1860-2000
    Topics: Chemistry and Pharmacology
    Notes: Summary A splitless Curie point pyrolysis inlet system for capillary columns has been built using conventional packed column apparatus. This has enabled the adsorption wire analysis system, for the rapid collection and direct GC analysis of vapours, to be used with capillary columns. Use of the technique for detecting traces of hydrocarbon fuels in arson investigation is described, as are problems occurring in its use.
    Type of Medium: Electronic Resource
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  • 3
    ISSN: 1052-9306
    Keywords: Chemistry ; Analytical Chemistry and Spectroscopy
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Chemistry and Pharmacology
    Notes: The difficulty of collecting volatile hydrocarbons, such as benzene, from street air in a form suitable for subsequent analysis is overcome by the use of a time-based elution procedure. By linking this technique to a gas chromatograph-mass spectrometer-data system, a rapid analysis is possible for low concentrations of collected material. Among advantages of this novel sample introduction procedure are the facility for collecting organic materials without interference from water vapour and their subsequent introduction into the g.c.-m.s. system without the use of any auxiliary solvents. Consequently the mass spectrometer can be used continuously on-line enabling the more volatile materials, normally masked by solvents, to be examined. This procedure is illustrated by the measurement of benzene and other hydrocarbon levels in street air (London). Following gas chromatographic separation the hydrocarbons can be identified by library search facilities attached to the mass spectrometer.
    Additional Material: 5 Ill.
    Type of Medium: Electronic Resource
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