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  • 1
    Electronic Resource
    Electronic Resource
    Copenhagen : International Union of Crystallography (IUCr)
    Applied crystallography online 13 (1980), S. 65-73 
    ISSN: 1600-5767
    Source: Crystallography Journals Online : IUCR Backfile Archive 1948-2001
    Topics: Geosciences , Physics
    Notes: The continuous Fourier transformation of I(h3) (h3 = 0,1) is proposed as a method for the analysis of the stacking sequence in close-packed structures. By this method, the diffraction pattern is directly translated into autocorrelation parameters P0n, P+n, P−n of the stacking sequence. It applies to periodic stacking sequences, for which the Fourier coefficients can be analysed in terms of the Zdhanov symbol, as well as to faulted stacking sequences, where the Fourier coefficients can be analysed in terms of faulting probabilities. In the work reported, the method proposed is applied to powder diffraction data from β′1 Cu–Al martensite. The stacking sequence in the martensite investigated can be dealt with as statistical, with Reichweite s = 3, and faulting parameters α = 0.18, β = 0.54. There is reasonably good agreement between the experimentally measured Fourier coefficients and the Fourier coefficients calculated from the above mentioned α and β values.
    Type of Medium: Electronic Resource
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  • 2
    ISSN: 1432-0827
    Keywords: Key words: Ewe — Ovariectomy — Calcitonin — Bone quality — Crystallography.
    Source: Springer Online Journal Archives 1860-2000
    Topics: Biology , Medicine , Physics
    Notes: Abstract. The aim of this study was to evaluate the effect of intermittent calcitonin on femoral bone quality in adult ewes from the time of ovariectomy. Six months after the start of the experiment, bone density measurements and mechanical testing (torsion and resonant frequency analysis of the diaphysis and compression of an excised trabecular bone cylinder from the femoral neck) were performed in sham-control and ovariectomized (OVX) ewes treated with placebo or salmon calcitonin (50 or 100 units, 3 times/week). Crystallinity of bone was evaluated by measuring X-ray diffraction line broadening. After OVX, a nonsignificant bone loss was found at all measured sites in the femur (−3 to −9%) together with a decreased biomechanical competence in the trabecular bone (compressive strain −28%, P 〈 0.05). Treatment with salmon calcitonin, 50 or 100 IU subcutaneously three times a week from the time of ovariectomy, resulted in a significant dose-dependent preservation of bone strength in the trabecular bone of the femoral neck compared with OVX. No adverse effects of calcitonin were observed on bone crystal composition as assessed by diffractiometry. We conclude that in adult ewes intermittent calcitonin treatment from the time of OVX was associated with a significant preservation of cancellous bone strength and strain in trabecular bone of the femoral neck, without affecting crystalline properties of bone.
    Type of Medium: Electronic Resource
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