ISSN:
1572-8854
Source:
Springer Online Journal Archives 1860-2000
Topics:
Geosciences
,
Physics
Notes:
Abstract The structure of the the title compound, C30H29NO, was determined by X-rays.M r =419.57, triclinic, space groupP1,a=5.8922(12),b=8.5855(11),c=12.2216(20) Å,α=78.145(12)°,β=79.181(15)°, γ=76.108(14)°,V c =581.1(1) Å3,Z=1,D x =1.199 Mg m−3. CuKα radiation (graphite crystal monochromator, λ=1.54184 Å),μ(CuKα)=5.17 cm−1,T=290K. Final conventionalR-factor=0.039,R w =0.042 for 2795 observed reflections and 377 variables. The structure was solved usingMultan andDirdif. With a view to determining the conformational preference of the piperidine ring when it is highly sustituted with a bulky group like the phenyl group, the present X-ray investigation was undertaken.
Type of Medium:
Electronic Resource
URL:
http://dx.doi.org/10.1007/BF01188189
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