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  • 1
    Electronic Resource
    Electronic Resource
    Springer
    International journal of fracture 14 (1978), S. 453-468 
    ISSN: 1573-2673
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Description / Table of Contents: Résumé Des expressions de compliance élastique pour des éprouvettes du type compacte (CT) et WOL ont été formulées pour une gamme large de longueurs de fissuration (a/W compris entre 0.2 et 0.975) en utilisant les résultats tirés de l'application des techniques modifiées de collationnement aux frontières selon Newman ainsi que de l'analyse d'une fissure profonde d'après Wilson. La localisation de l'axe de rotation des bras de l'éprouvette pour différents longueurs de fissure a été calculée et utilisée en conséquence dans une technique d'extrapolation proposée pour prédire la compliance à toutes localisations de l'éprouvette convenant pour la mesure de la déflection durant un essai de croissance de fissure. Les compliances prédites ont été trouvées en excellent accord avec les valeurs expérimentales pour les deux types d'éprouvette considérés. Les expressions de compliance ont également été formulées pour un éprouvette de traction à fissure centrale.
    Notes: Abstract Elastic compliance expressions for compact type (CT) and WOL specimens have been formulated for a wide range of crack lengths (0.2 ⩽a/W ⩽ 0.975) using results from Newman's modified boundary collection techniques and Wilson's deep crack analysis. The location of the axis of rotation of the specimen arms at various crack lengths has been calculated and subsequently used in a proposed extrapolation technique to predict compliance at any location of the specimen convenient for measuring deflection during a crack growth test. The predicted compliances were found to be in excellent agreement with expreimental values for the two specimen types considered. Compliance expressions are also included for the center crack tension specimen.
    Type of Medium: Electronic Resource
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  • 2
    ISSN: 1573-2673
    Source: Springer Online Journal Archives 1860-2000
    Topics: Mechanical Engineering, Materials Science, Production Engineering, Mining and Metallurgy, Traffic Engineering, Precision Mechanics
    Description / Table of Contents: Résumé Les nombreuses situations pratiques où l'amorçage d'une croissance rapide d'une fissure ne peut être formellement prévue, et où les conséquences d'une rupture à grande échelle seraient catastrophiques, requièrent le développement et l'usage de la technique de mécanique de la rupture du point de vue de l'arrêt de fissuration. La plupart des procédures actuelles recourent à des analyses linéaires et élastique et aux caractérisations correspondantes des propriétés de résistance à la rupture des matériaux. Même si la base théorique pour une approche de ce niveau est encore incomplète, des applications pratiques spécifiques peuvent en être faites, ainsi qu'on le décrit dans l'étude. En outre, pour répondre aux déficiences actuelles, et pour traiter les conditions qui ne peuvent s'accomoder des conditions de plastification à petite échelle, on développe une analyse dynamique viscoplastique plus évoluée. Dans l'étude, on décrit une approche qui associe des essais de propagation de fissure dûment instrumentés et des simulations dynamiques viscoplastiques par éléments finis. Cette approche, qui est déjà utilisée pour établir les valeurs critiques du paramètres T * développé par Atluri pour caractériser l'extrémité de la fissure, est approfondie en vue de fournir des valeurs transférables de la ténacité du matériau vis-à-vis de l'arrêt de propagation d'une fissure, là où prédominent des conditions de viscoplasticité dynamique.
    Notes: Abstract The many practical situations in which the initiation of rapid crack propagation cannot be absolutely precluded and where the consequences of a large scale fracture would be catastrophic mandate the development and use of crack arrest fracture mechanics technology. Most currently applied procedures utilize linear elastic analyses and corresponding material fracture property characterizations. Even though the theoretical basis for the use of this level of approach is incomplete, selected practical applications are described in this paper that show that these can still be effectively made. In addition, to address the current deficiencies and to treat those conditions where small-scale yielding conditions are clearly not satisfied, more advanced viscoplastic-dynamic analyses are also being developed. An approach is described in this paper that performs well-instrumented fracture propagation experiments in concert with viscoplastic dynamic finite-element simulations. This approach, currently used to quantify critical values of the T * crack tip characterizing parameter developed by Atluri, is being pursued in order to provide transferable material crack arrest toughness values in the regime where viscoplastic-dynamic conditions dominate.
    Type of Medium: Electronic Resource
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  • 3
    Electronic Resource
    Electronic Resource
    Chichester [u.a.] : Wiley-Blackwell
    Surface and Interface Analysis 15 (1990), S. 167-172 
    ISSN: 0142-2421
    Keywords: Chemistry ; Polymer and Materials Science
    Source: Wiley InterScience Backfile Collection 1832-2000
    Topics: Physics
    Notes: X-ray photoelectron spectroscopy (XPS) has been used to study the interphase between a model anaerobic adhesive system composed of triethylene glycol dimethacrylate monomer (TRIEGMA) and a curing system consisting of cumene hydroperoxide (CHP), acetylphenyl hydrazine (APH) and saccharin (BS), and the substrates copper, iron, zinc and aluminum. Miniature cantilever beam specimens were prepared by curing beams of the adhesive against beams of the metal substrates. The specimens were then immersed in liquid nitrogen, causing the adhesive to delaminate from the substrate. XPS spectra obtained from the adhesive failure surfaces were very similar to spectra obtained from the bulk adhesive, containing peaks corresponding to carbon, oxygen and trace amounts of sulfur and nitrogen. However, the spectra also contained peaks due to trace amounts of metal or metal ions from the substrate. Spectra obtained from the substrate failure surfaces were very different from those of the corresponding adhesive failure surfaces and contained peaks due to higher concentrations of metal or metal ions and higher concentrations of nitrogen and sulfur, indicating that failure was near the interface and that both BS and APH segregated to the interface. C 1s multiplex spectra obtained from thin films of BS spin-coated from dilute solutions onto iron, copper and zinc contained a weak component shifted from the main hydrocarbon peak to higher binding energy by ∼3.1 eV. This was more similar to the shift observed from the hydrated sodium salt of BS (Δ2.9 eV) than neat BS (δ3.7 eV), indicating that BS readily forms a complex with these substrates. When a copper foil was placed in a solution of BS and analyzed periodically in XPS, peaks due to Cu(I) were initially observed in the Cu 2p spectra, but peaks due to Cu(II) appeared after ∼110 h. The Cu(II) BS complex was also observed when a blue powder, which precipitated when a copper foil was placed in a solution of BS in methanol, was analyzed. Spectra obtained from aluminum (which does not catalyze the polymerization of the anaerobic adhesive as well as copper or iron) did not show the formation of a BS-metal complex in any of the samples studied.
    Additional Material: 4 Ill.
    Type of Medium: Electronic Resource
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