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  • 2005-2009  (3)
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  • 1
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Solid state phenomena Vol. 118 (Dec. 2006), p. 137-142 
    ISSN: 1662-9779
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Physics
    Notes: In a previous study, an aluminum nitride (AlN) layer was formed below the melting pointof aluminum (Al) on the surface of an Al substrate (JIS-A1050) in a barrel withalumina/aluminum-magnesium alloy powder which activates the substrate in the nitrogenatmosphere. In this study, the mechanism of formation of AlN in the barrel was examined. AlNformation requires an incubation period. During the incubation period, a white region on the surfaceis observed by the optical microscopy. The Electron Probe Micro Analyzer (EPMA) show that thisregion contains magnesium (Mg). It seems that Mg penetrates and diffuses from the filled Al-Mgpowder in the barrel. After that, the nitride is partially generated at the surface of the Al substrate,and it grows with the substrate surface. The AlN layer thickness increases proportionally with thesquare root of time, and it has good adhesion
    Type of Medium: Electronic Resource
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  • 2
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Solid state phenomena Vol. 118 (Dec. 2006), p. 97-102 
    ISSN: 1662-9779
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Physics
    Notes: Acetylene and ethylene are frequently used in vacuum carburizing in Japan. In this studythe natural gas which is available from the lifeline is applied to vacuum carburizing. The gascomposition inside the furnace was analyzed by the gas chromatography in order to examine thecarbon infiltration mechanism. Unsaturated hydrocarbon gases (such as acetylene and ethylene) aregenerated from the natural gas. The effect of acetylene concentration in the furnace on the carboninfiltration rate was investigated. The carbon amount which infiltrates into the steel increases, asacetylene concentration in furnace increases. It is possible that carbon concentration of specimensurface increases to the cementite precipitation concentration in the short term, when natural gasflow rate increases in the initial carburizing stage. After that, carbon concentration of specimensurface does not decrease, even if the natural gas flow decreases, because carbon atoms which areconsumed for diffusion to inside are sufficiently supplied. By using this method, inhibition of sootgeneration, reduction of process gas and shortening of the carburizing period are possible. Thecarbon concentration profile of the vacuum carburized specimen was compared with the simulation
    Type of Medium: Electronic Resource
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  • 3
    Electronic Resource
    Electronic Resource
    s.l. ; Stafa-Zurich, Switzerland
    Solid state phenomena Vol. 141-143 (July 2008), p. 499-504 
    ISSN: 1662-9779
    Source: Scientific.Net: Materials Science & Technology / Trans Tech Publications Archiv 1984-2008
    Topics: Physics
    Notes: The effect of reheating to the semisolid state (soaking treatment) on the microstructureevolution of the A356 aluminum alloy prepared by ultrasonic melt treatment was studied in thispaper. The results showed that in general the longer the soaking process the larger and the moreround the grains obtained. Higher roundness occurs at shorter soaking times in the fine-grained ascastsamples, and at longer times in the inhomogeneous or the coarser-grained as-cast structures.The optimum thixotropic condition (high roundness, 0.72, and small globule sizes 〈 90 μm) areachieved after 5 min. soaking in the samples treated by UST at 623 and 620oC, which is the typicalsoaking time dictated by the industrial practice in SSM. The amount of entrapped eutectic asobserved after soaking treatments is uniquely very small, suggesting that the UST-treated ingots willhave better formability in the semisolid state. The growth rate constants are substantially low: in theorder of 479-748 μm3/s. These growth rate constants are much lower than those reported for MHDcastA356 ingots. The growth rates of the samples produced by UST in the liquid state (i.e., 626,623 and 620oC. Note that liquidus temperature is 619oC) are lower than those of the samples treatedin the semi-solid temperatures, i.e., 617 and 614oC. The Ostwald ripening is most likely thedominant growth mechanism in the UST-treated samples during the soaking treatments. Theseresults reveal the feasibility and competence of UST as a potential route for thixotropic feedstockproduction
    Type of Medium: Electronic Resource
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